(VO)2(Br₂C₆O₄)(C₁₂H₇ClN₂)2⁽²⁺⁾*SO₄^(2-)=[(VO)2(Br₂C₆O₄)(C₁₂H₇ClN₂)2](SO₄)

Base Information

Chemical Name:(VO)2(Br₂C₆O₄)(C₁₂H₇ClN₂)2⁽²⁺⁾*SO₄^(2-)=[(VO)2(Br₂C₆O₄)(C₁₂H₇ClN₂)2](SO₄)
CAS No.:230953-51-2
Molecular Formula:C₃₀H₁₄Br₂Cl₂N₄O₆V₂*O₄S
Molecular Weight:955.125
Hs Code.:

(VO)2(Br<sub>2</sub>C<sub>6</sub>O<sub>4</sub>)(C<sub>12</sub>H<sub>7</sub>ClN<sub>2</sub>)2<sup>(2+)</sup>*SO<sub>4</sub><sup>(2-)</sup>=[(VO)2(Br<sub>2</sub>C<sub>6</sub>O<sub>4</sub>)(C<sub>12</sub>H<sub>7</sub>ClN<sub>2</sub>)2](SO<sub>4</sub>)

Synonyms:(VO)2(Br₂C₆O₄)(C₁₂H₇ClN₂)2⁽²⁺⁾*SO₄^(2-)=[(VO)2(Br₂C₆O₄)(C₁₂H₇ClN₂)2](SO₄)

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Chemical Property of (VO)2(Br₂C₆O₄)(C₁₂H₇ClN₂)2⁽²⁺⁾*SO₄^(2-)=[(VO)2(Br₂C₆O₄)(C₁₂H₇ClN₂)2](SO₄)

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Technology Process of (VO)2(Br₂C₆O₄)(C₁₂H₇ClN₂)2⁽²⁺⁾*SO₄^(2-)=[(VO)2(Br₂C₆O₄)(C₁₂H₇ClN₂)2](SO₄)

There total 1 articles about (VO)2(Br₂C₆O₄)(C₁₂H₇ClN₂)2⁽²⁺⁾*SO₄^(2-)=[(VO)2(Br₂C₆O₄)(C₁₂H₇ClN₂)2](SO₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: vanadyl(IV) sulphate pentahydrate

: 4199-89-7
5-Chloro-1,10-phenanthroline

: 4370-59-6
bromanilic acid

: 230953-51-2
(VO)2(Br₂C₆O₄)(C₁₂H₇ClN₂)2⁽²⁺⁾*SO₄^(2-)=[(VO)2(Br₂C₆O₄)(C₁₂H₇ClN₂)2](SO₄)

: 7664-93-9
sulfuric acid

Guidance literature:: In methanol; dropwise addn. of soln. of VOSO4 to soln of bromanilic acid, addn. of soln. of N-ligand (stirring, room temp.), refluxing (8 h; crystn.); filtration, washing (MeOH, Et2O), drying (vac., over P2O5), recrystn. (DMF/EtOH); elem. anal.;
DOI:10.1080/00945719909349506