C₅₄H₉₂N₆O₁₁Si₄

Base Information

Chemical Name:C₅₄H₉₂N₆O₁₁Si₄
CAS No.:1579198-19-8
Molecular Formula:C₅₄H₉₂N₆O₁₁Si₄
Molecular Weight:1113.7
Hs Code.:

C<sub>54</sub>H<sub>92</sub>N<sub>6</sub>O<sub>11</sub>Si<sub>4</sub>

Synonyms:C₅₄H₉₂N₆O₁₁Si₄

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Chemical Property of C₅₄H₉₂N₆O₁₁Si₄

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Technology Process of C₅₄H₉₂N₆O₁₁Si₄

There total 15 articles about C₅₄H₉₂N₆O₁₁Si₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1579198-21-2
C₄₂H₆₄N₆O₁₁Si₂

: 79271-56-0
triethylsilyl trifluoromethyl sulfonate

: 1579198-19-8
C₅₄H₉₂N₆O₁₁Si₄

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1021/ja501460j

Reference yield:

: 1579198-10-9
C₃₁H₂₅N₃O₇

: 1579198-19-8
C₅₄H₉₂N₆O₁₁Si₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: dichloromethane / 1 h / 20 °C / Inert atmosphere; Molecular sieve

1.2: 2 h / Inert atmosphere; Molecular sieve

2.1: ethanol; water / 8 h / 20 - 90 °C / Inert atmosphere

3.1: pyridine / 1.5 h / 20 °C / Inert atmosphere

4.1: triphenylphosphine; silica gel; water / tetrahydrofuran / 4 h / 20 - 50 °C / Inert atmosphere

5.1: N-ethyl-N,N-diisopropylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

6.1: triethylamine / dichloromethane / 5 h / 20 °C / Inert atmosphere

With pyridine; water; silica gel; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/ja501460j

Reference yield:

: 1579198-15-4
C₂₆H₂₄N₈O₅

: 1579198-19-8
C₅₄H₉₂N₆O₁₁Si₄

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 1.5 h / 20 °C / Inert atmosphere

2: triphenylphosphine; silica gel; water / tetrahydrofuran / 4 h / 20 - 50 °C / Inert atmosphere

3: N-ethyl-N,N-diisopropylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

4: triethylamine / dichloromethane / 5 h / 20 °C / Inert atmosphere

With pyridine; water; silica gel; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja501460j