C₅₇H₈₇N₃O₁₇S

Base Information

Chemical Name:C₅₇H₈₇N₃O₁₇S
CAS No.:122825-77-8
Molecular Formula:C₅₇H₈₇N₃O₁₇S
Molecular Weight:1118.39
Hs Code.:

C<sub>57</sub>H<sub>87</sub>N<sub>3</sub>O<sub>17</sub>S

Synonyms:C₅₇H₈₇N₃O₁₇S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₇H₈₇N₃O₁₇S

Chemical Property:

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Technology Process of C₅₇H₈₇N₃O₁₇S

There total 13 articles about C₅₇H₈₇N₃O₁₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 122825-63-2
3-O-acetyl-23-O-demycinosyl-4''-O-isovaleryl-23-O-phenylacetyltylosin

: 26494-76-8
4-amino-4H-tetrahydro-1,4-thiazine-1,1-dioxide

: 122825-77-8
C₅₇H₈₇N₃O₁₇S

Guidance literature:: In tetrahydrofuran; at 25 ℃; for 50h;
DOI:10.1039/P19890000787

Reference yield:

: 1468-39-9
Isovaleric anhydride

: 122825-77-8
C₅₇H₈₇N₃O₁₇S

Guidance literature:: Multi-step reaction with 8 steps

1: 49 percent / 4-dimethylaminopyridine, triethylamine / CH₂Cl₂ / 18 h / 25 °C

2: 82 percent / 4-dimethylaminopyridine, triethylamine / CH₂Cl₂ / 21 h / 25 °C

3: 45 percent / triethylamine (33percent) / methanol / 66 h / 25 °C

4: 87 percent / acetone / 18 h / 25 °C

5: 70 percent / N-(3-dimethylaminopropyl)-N'-ethylcarbodi-imide hydrochloride, pyridine, TFA / dimethylsulfoxide / 36 h / 25 °C

6: 89 percent / pyridine / CH₂Cl₂ / 41 h / -7 °C

7: 90 percent / methanol / 7 h / 50 °C

8: 89 percent / tetrahydrofuran / 50 h / 25 °C

With pyridine; methanol; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; acetone;
DOI:10.1039/P19890000787

Reference yield:

: 69988-46-1
2'-O-acetyltylosin

: 122825-77-8
C₅₇H₈₇N₃O₁₇S

Guidance literature:: Multi-step reaction with 9 steps

1: 49 percent / 4-dimethylaminopyridine, pyridine / CH₂Cl₂ / 47 h / 25 °C

2: 49 percent / 4-dimethylaminopyridine, triethylamine / CH₂Cl₂ / 18 h / 25 °C

3: 82 percent / 4-dimethylaminopyridine, triethylamine / CH₂Cl₂ / 21 h / 25 °C

4: 45 percent / triethylamine (33percent) / methanol / 66 h / 25 °C

5: 87 percent / acetone / 18 h / 25 °C

6: 70 percent / N-(3-dimethylaminopropyl)-N'-ethylcarbodi-imide hydrochloride, pyridine, TFA / dimethylsulfoxide / 36 h / 25 °C

7: 89 percent / pyridine / CH₂Cl₂ / 41 h / -7 °C

8: 90 percent / methanol / 7 h / 50 °C

9: 89 percent / tetrahydrofuran / 50 h / 25 °C

With pyridine; methanol; dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; dimethyl sulfoxide; acetone;
DOI:10.1039/P19890000787