tetrabenzoyl mannosyl pentenate

Base Information

• Chemical Name: tetrabenzoyl mannosyl pentenate
• CAS No.: 920749-11-7
• Molecular Formula: C₃₉H₃₄O₁₁
• Molecular Weight: 678.692
• Mol file: 920749-11-7.mol

Synonyms:tetrabenzoyl mannosyl pentenate

Chemical Property of tetrabenzoyl mannosyl pentenate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tetrabenzoyl mannosyl pentenate

There total 1 articles about tetrabenzoyl mannosyl pentenate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

pent-4-enoic acid (591-80-0) + 2,3,4,6-tetra-O-benzoyl-α,β-D-mannospyranose (627466-98-2) → tetrabenzoyl mannosyl pentenate (920749-11-7)

Guidance literature:

With dacarbazine; dmap; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1016/j.tetlet.2006.10.158

Reference yield: 90.0%

tetrabenzoyl mannosyl pentenate (920749-11-7) + methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside (19488-48-3) → methyl-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranoside (128503-40-2)

Guidance literature:

tetrabenzoyl mannosyl pentenate; With Phenylselenyl bromide; silver trifluoromethanesulfonate; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at -78 ℃; for 0.25h;

methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside; In dichloromethane; at -78 ℃; for 0.333333h;

DOI:10.1016/j.tetlet.2006.10.158

Reference yield: 87.0%

tetrabenzoyl mannosyl pentenate (920749-11-7) + methyl 2,3,6-tri-O-benzyl-α-D-mannopyranoside (19488-48-3,19488-49-4,51842-16-1,55697-49-9,115414-37-4,95475-33-5) → methyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-mannopyranoside

Guidance literature:

tetrabenzoyl mannosyl pentenate; With Phenylselenyl bromide; silver trifluoromethanesulfonate; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at -78 ℃; for 0.25h;

methyl 2,3,6-tri-O-benzyl-α-D-mannopyranoside; In dichloromethane; at -78 ℃; for 0.333333h;

DOI:10.1016/j.tetlet.2006.10.158

upstream raw materials:

pent-4-enoic acid

2,3,4,6-tetra-O-benzoyl-α,β-D-mannospyranose

Downstream raw materials:

methyl-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-α-D-glucopyranoside