2-acetamido-3-O-(2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-(6''-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranosyl azide

Base Information

Chemical Name:2-acetamido-3-O-(2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-(6''-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranosyl azide
CAS No.:169393-73-1
Molecular Formula:C₅₅H₆₄N₄O₁₄
Molecular Weight:1005.13
Hs Code.:

Synonyms:2-acetamido-3-O-(2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-(6''-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranosyl azide

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Chemical Property of 2-acetamido-3-O-(2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-(6''-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranosyl azide

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Technology Process of 2-acetamido-3-O-(2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-(6''-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranosyl azide

There total 2 articles about 2-acetamido-3-O-(2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-(6''-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranosyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 2-acetamido-3-O-(2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-(2'',3'',4''-tri-O-acetyl-6''-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranosyl azide

: 169393-73-1
2-acetamido-3-O-(2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-(6''-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranosyl azide

Guidance literature:: With sodium methylate; In methanol; at 20 ℃; for 5h;
DOI:10.1016/j.carres.2006.09.012

Reference yield:

: 169393-72-0
2,3,4-tri-O-acetyl-6-O-benzyl-α,β-D-galactopyranosyl trichloroacetimidate

: N-[(2R,3R,4R,5S,6R)-2-Azido-6-benzyloxymethyl-5-hydroxy-4-((2S,3S,4R,5R,6S)-3,4,5-tris-benzyloxy-6-methyl-tetrahydro-pyran-2-yloxy)-tetrahydro-pyran-3-yl]-acetamide

: 169393-73-1
2-acetamido-3-O-(2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-(6''-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranosyl azide

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; Amberlite H(+) IR 120; sodium methylate; Yield given. Multistep reaction; 1.) CH₂Cl₂, 2.) MeOH;

Reference yield: 59.0%

: 169393-73-1
2-acetamido-3-O-(2',3',4'-tri-O-benzyl-α-L-fucopyranosyl)-6-O-benzyl-2-deoxy-4-O-(6''-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranosyl azide

: (4S,5R,6R)-4-Acetoxy-5-acetylamino-2-ethylsulfanyl-6-((1S,2R)-1,2,3-triacetoxy-propyl)-tetrahydro-pyran-2-carboxylic acid methyl ester

: C₂₀H₂₇O₁₂NC₂₁H₂₂OC₁₉H₂₂O₈C₆H₁₂O₄N₄C₂H₂OC₇H₆

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In acetonitrile; at -28 ℃; for 14h;
DOI:10.1016/j.carres.2006.09.012