C₂₂H₃₁NO₃

Base Information

Chemical Name:C₂₂H₃₁NO₃
CAS No.:1412947-64-8
Molecular Formula:C₂₂H₃₁NO₃
Molecular Weight:357.493
Hs Code.:

C<sub>22</sub>H<sub>31</sub>NO<sub>3</sub>

Synonyms:C₂₂H₃₁NO₃

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Chemical Property of C₂₂H₃₁NO₃

Chemical Property:

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Technology Process of C₂₂H₃₁NO₃

There total 10 articles about C₂₂H₃₁NO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1412947-76-2
C₂₂H₃₃NO₃

: 1412947-64-8
C₂₂H₃₁NO₃

Guidance literature:: With pyridine; N-chloro-succinimide; In chloroform; at 20 - 60 ℃; for 6h;
DOI:10.1039/c2cc36260k

Reference yield:

: 1412947-59-1
C₂₀H₂₈O₄

: 1412947-64-8
C₂₂H₃₁NO₃

Guidance literature:: Multi-step reaction with 9 steps

1.1: chloro-trimethyl-silane; pyridine / tetrahydrofuran / -78 °C

1.2: -78 - 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 14 h / 0 - 20 °C / Reflux

3.1: triethylamine / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

4.1: sodium iodide / butanone / 24 h / Reflux

5.1: copper(l) iodide; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / -40 °C

5.2: 0 - 20 °C

6.1: AD-mix β; water / tert-butyl alcohol / 0 - 5 °C

7.1: sodium periodate / tert-butyl alcohol; water / 0 - 20 °C

8.1: triethylamine; hydroxylamine hydrochloride / ethanol / 0 - 20 °C

9.1: pyridine; N-chloro-succinimide / chloroform / 6 h / 20 - 60 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium periodate; N-chloro-succinimide; copper(l) iodide; lithium aluminium tetrahydride; chloro-trimethyl-silane; AD-mix β; hydroxylamine hydrochloride; water; triethylamine; sodium iodide; In tetrahydrofuran; ethanol; dichloromethane; chloroform; water; butanone; tert-butyl alcohol;
DOI:10.1039/c2cc36260k

Reference yield:

: 88920-24-5
p-methoxybenzyloxy acetic acid

: 1412947-64-8
C₂₂H₃₁NO₃

Guidance literature:: Multi-step reaction with 10 steps

1.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

2.1: chloro-trimethyl-silane; pyridine / tetrahydrofuran / -78 °C

2.2: -78 - 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 14 h / 0 - 20 °C / Reflux

4.1: triethylamine / dichloromethane / 5 h / 0 - 20 °C / Inert atmosphere

5.1: sodium iodide / butanone / 24 h / Reflux

6.1: copper(l) iodide; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / -40 °C

6.2: 0 - 20 °C

7.1: AD-mix β; water / tert-butyl alcohol / 0 - 5 °C

8.1: sodium periodate / tert-butyl alcohol; water / 0 - 20 °C

9.1: triethylamine; hydroxylamine hydrochloride / ethanol / 0 - 20 °C

10.1: pyridine; N-chloro-succinimide / chloroform / 6 h / 20 - 60 °C

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; sodium periodate; N-chloro-succinimide; copper(l) iodide; lithium aluminium tetrahydride; chloro-trimethyl-silane; AD-mix β; hydroxylamine hydrochloride; water; triethylamine; dicyclohexyl-carbodiimide; sodium iodide; In tetrahydrofuran; ethanol; dichloromethane; chloroform; water; butanone; tert-butyl alcohol;
DOI:10.1039/c2cc36260k