(1S,3R)-2,2-dimethyl-3-(2-(2-methyl-1,3-dioxolan-2-yl)ethyl)-4-methylenecyclohexanol

Base Information

Chemical Name:(1S,3R)-2,2-dimethyl-3-(2-(2-methyl-1,3-dioxolan-2-yl)ethyl)-4-methylenecyclohexanol
CAS No.:1020736-17-7
Molecular Formula:C₁₅H₂₆O₃
Molecular Weight:254.37
Hs Code.:

Synonyms:(1S,3R)-2,2-dimethyl-3-(2-(2-methyl-1,3-dioxolan-2-yl)ethyl)-4-methylenecyclohexanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,3R)-2,2-dimethyl-3-(2-(2-methyl-1,3-dioxolan-2-yl)ethyl)-4-methylenecyclohexanol

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Technology Process of (1S,3R)-2,2-dimethyl-3-(2-(2-methyl-1,3-dioxolan-2-yl)ethyl)-4-methylenecyclohexanol

There total 5 articles about (1S,3R)-2,2-dimethyl-3-(2-(2-methyl-1,3-dioxolan-2-yl)ethyl)-4-methylenecyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1123890-01-6
C₁₇H₂₈O₄

: 1020736-17-7
(1S,3R)-2,2-dimethyl-3-(2-(2-methyl-1,3-dioxolan-2-yl)ethyl)-4-methylenecyclohexanol

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 7h; optical yield given as %ee;
DOI:10.1002/adsc.200700511

Reference yield: 77.0%

: 32247-48-6
2-methyl-2-((E)-4-methyl-6-(3,3-dimethyloxiran-2-yl)hex-3-enyl)-1,3-dioxolane

: 1020736-17-7
(1S,3R)-2,2-dimethyl-3-(2-(2-methyl-1,3-dioxolan-2-yl)ethyl)-4-methylenecyclohexanol

Guidance literature:: With 2,4,6-trimethyl-pyridine; bis(cyclopentadienyl)titanium dichloride; manganese; tertiary butyl chloride; In tetrahydrofuran; for 2h;
DOI:10.1021/ol800326n

Reference yield:

: C₁₅H₂₆O₃

: 1020736-17-7
(1S,3R)-2,2-dimethyl-3-(2-(2-methyl-1,3-dioxolan-2-yl)ethyl)-4-methylenecyclohexanol

: 1123890-03-8
C₁₅H₂₆O₃

Guidance literature:: With 2,4,6-trimethyl-pyridine; bis(cyclopentadienyl)titanium dichloride; manganese; chloro-trimethyl-silane; In tetrahydrofuran; at 20 ℃; for 1.5h; optical yield given as %ee; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/adsc.200700511