4-nitro-N-(3-methylbut-2-en-1-yl)-N-(prop-2-yn-1-yl)benzenesulfonamide

Base Information

• Chemical Name: 4-nitro-N-(3-methylbut-2-en-1-yl)-N-(prop-2-yn-1-yl)benzenesulfonamide
• CAS No.: 1147121-55-8
• Molecular Formula: C₁₄H₁₆N₂O₄S
• Molecular Weight: 308.358

Synonyms:4-nitro-N-(3-methylbut-2-en-1-yl)-N-(prop-2-yn-1-yl)benzenesulfonamide

Chemical Property of 4-nitro-N-(3-methylbut-2-en-1-yl)-N-(prop-2-yn-1-yl)benzenesulfonamide

Chemical Property:

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Technology Process of 4-nitro-N-(3-methylbut-2-en-1-yl)-N-(prop-2-yn-1-yl)benzenesulfonamide

There total 1 articles about 4-nitro-N-(3-methylbut-2-en-1-yl)-N-(prop-2-yn-1-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

prenyl bromide (870-63-3) + 4-nitro-N-(prop-2-yn-1-yl)benzene-1-sulfonamide (221101-01-5) → 4-nitro-N-(3-methylbut-2-en-1-yl)-N-(prop-2-yn-1-yl)benzenesulfonamide (1147121-55-8)

Guidance literature:

With potassium carbonate; In acetone; at 55 ℃; for 16h;

DOI:10.1021/jacs.5b09311

Reference yield: 73.0%

4-nitro-N-(3-methylbut-2-en-1-yl)-N-(prop-2-yn-1-yl)benzenesulfonamide (1147121-55-8) → N-[(3,3-dimethyloxiran-2-yl)methyl]-4-nitro-N-(prop-2-ynyl)benzenesulfonamide (1147121-35-4)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; water; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.tet.2009.01.065

Reference yield: 42.0%

4-nitro-N-(3-methylbut-2-en-1-yl)-N-(prop-2-yn-1-yl)benzenesulfonamide (1147121-55-8) → 3-methylene-4-(1-methylethenyl)-1-[(4-nitrophenyl)sulfonyl]-pyrrolidine (1201807-68-2)

Guidance literature:

With bismuth(III) chloride; In 1,2-dichloro-ethane; at 60 ℃; for 12h; Inert atmosphere;

DOI:10.1002/ejoc.200900819

upstream raw materials:

prenyl bromide

4-nitro-N-(prop-2-yn-1-yl)benzene-1-sulfonamide

Downstream raw materials:

N-[(3,3-dimethyloxiran-2-yl)methyl]-4-nitro-N-(prop-2-ynyl)benzenesulfonamide

3-methylene-4-(1-methylethenyl)-1-[(4-nitrophenyl)sulfonyl]-pyrrolidine

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