C₄₈H₈₈O₉Si₃

Base Information

Chemical Name:C₄₈H₈₈O₉Si₃
CAS No.:1422463-34-0
Molecular Formula:C₄₈H₈₈O₉Si₃
Molecular Weight:893.478
Hs Code.:

C<sub>48</sub>H<sub>88</sub>O<sub>9</sub>Si<sub>3</sub>

Synonyms:C₄₈H₈₈O₉Si₃

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Chemical Property of C₄₈H₈₈O₉Si₃

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Technology Process of C₄₈H₈₈O₉Si₃

There total 24 articles about C₄₈H₈₈O₉Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1033588-06-5
C₂₂H₄₀O₄Si

: 1422462-85-8
C₂₆H₄₈O₅Si₂

: 1422463-34-0
C₄₈H₈₈O₉Si₃

Guidance literature:: C₂₆H₄₈O₅Si₂; With lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.333333h; Inert atmosphere;

C₂₂H₄₀O₄Si; In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.333333h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo3026077

Reference yield:

: C₂₉H₄₈O₅Si

: 1422463-34-0
C₄₈H₈₈O₉Si₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; sodium periodate / tetrahydrofuran; diethyl ether / 2 h / 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran; diethyl ether / 0.33 h / -78 °C / Inert atmosphere

2.2: 0.33 h / -78 °C / Inert atmosphere

With sodium periodate; water; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether;
DOI:10.1021/jo3026077

Reference yield:

: 1422463-22-6
C₁₆H₂₂O₃

: 1422463-34-0
C₄₈H₈₈O₉Si₃

Guidance literature:: Multi-step reaction with 16 steps

1.1: diisobutylaluminium hydride / dichloromethane / 1 h / -78 °C / Inert atmosphere

2.1: 1H-imidazole / N,N-dimethyl-formamide / 1 h / 20 °C / Inert atmosphere

3.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 20 °C / pH 7

3.2: 1 h / 20 °C / Inert atmosphere

4.1: toluene / 16 h / 112 °C / Inert atmosphere; Sealed tube; High pressure

5.1: sodium hydride / 1,2-dimethoxyethane / 1 h / 20 °C / Inert atmosphere

5.2: 3 h / Inert atmosphere; Reflux

6.1: diisobutylaluminium hydride / tetrahydrofuran; toluene / 1.5 h / -78 °C / Inert atmosphere

7.1: L-(+)-diisopropyl tartrate; titanium(IV) isopropylate; tert.-butylhydroperoxide / dichloromethane; decane / -78 - -50 °C / Molecular sieve; Inert atmosphere

8.1: sodium bis(2-methoxyethoxy)aluminium dihydride / tetrahydrofuran; toluene / 2.5 h / 0 °C / Inert atmosphere

9.1: pyridine / dichloromethane / 3 h / Inert atmosphere

10.1: camphor-10-sulfonic acid / dichloromethane; ethanol / 1.5 h / 0 °C / Inert atmosphere

11.1: pyridine / dichloromethane / 1.5 h / Inert atmosphere

12.1: ammonium hydroxide; water / dichloromethane; ethanol / 1 h / 20 °C

13.1: triethylamine / dichloromethane / 0.33 h / -78 °C / Inert atmosphere

14.1: water; acetic acid / tetrahydrofuran / 1.5 h / 0 °C

15.1: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 1 h / 20 °C / Inert atmosphere

16.1: lithium diisopropyl amide / tetrahydrofuran; diethyl ether / 0.33 h / -78 °C / Inert atmosphere

16.2: 0.33 h / -78 °C / Inert atmosphere

With pyridine; 1H-imidazole; titanium(IV) isopropylate; tert.-butylhydroperoxide; ammonium hydroxide; L-(+)-diisopropyl tartrate; camphor-10-sulfonic acid; water; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; acetic acid; triethylamine; sodium bis(2-methoxyethoxy)aluminium dihydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; lithium diisopropyl amide; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; decane; ethanol; dichloromethane; N,N-dimethyl-formamide; toluene; 3.2: |Dess-Martin Oxidation / 4.1: |Wittig Olefination / 5.1: |Horner-Wadsworth-Emmons Olefination / 5.2: |Horner-Wadsworth-Emmons Olefination / 7.1: |Sharpless Asymmetric Epoxidation / 15.1: |Dess-Martin Oxidation;
DOI:10.1021/jo3026077