C₆₉H₁₃₂O₂₅

Base Information

Chemical Name:C₆₉H₁₃₂O₂₅
CAS No.:1424713-04-1
Molecular Formula:C₆₉H₁₃₂O₂₅
Molecular Weight:1361.79
Hs Code.:

C<sub>69</sub>H<sub>132</sub>O<sub>25</sub>

Synonyms:C₆₉H₁₃₂O₂₅

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Chemical Property of C₆₉H₁₃₂O₂₅

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Technology Process of C₆₉H₁₃₂O₂₅

There total 18 articles about C₆₉H₁₃₂O₂₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1424713-02-9
C₆₉H₁₁₆O₉

: 1424713-04-1
C₆₉H₁₃₂O₂₅

Guidance literature:: With osmium(VIII) oxide; water; 4-methylmorpholine N-oxide; In acetone; tert-butyl alcohol; at 0 - 20 ℃; for 24h;
DOI:10.1055/s-0032-1317929

Reference yield:

: 1424712-78-6
C₂₄H₄₄O₅

: 1424713-04-1
C₆₉H₁₃₂O₂₅

Guidance literature:: Multi-step reaction with 9 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / -10 °C / Inert atmosphere

2.1: sodium; methanol / 1 h / 0 - 20 °C / Inert atmosphere

3.1: pyridine / 72 h / 110 °C

4.1: potassium carbonate; palladium 10% on activated carbon; hydrogen / ethyl acetate / 48 h / 20 °C / 760.05 Torr

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

6.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

6.2: 0 - 20 °C / Inert atmosphere

7.1: acetic acid / methanol / 48 h / 20 °C

8.1: water; sodium hydroxide; tetra-(n-butyl)ammonium iodide / toluene / 48 h / 45 °C

8.2: 1 h / 0 °C / Inert atmosphere

8.3: 12 h / 0 - 20 °C / Inert atmosphere

9.1: water; osmium(VIII) oxide; 4-methylmorpholine N-oxide / acetone; tert-butyl alcohol / 24 h / 0 - 20 °C

With pyridine; methanol; osmium(VIII) oxide; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; water; hydrogen; sodium; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; acetic acid; 4-methylmorpholine N-oxide; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; mineral oil; tert-butyl alcohol; 1.1: |Mitsunobu Displacement / 6.2: |Williamson Ether Synthesis / 8.3: |Williamson Ether Synthesis;
DOI:10.1055/s-0032-1317929

Reference yield:

: C₂₂H₄₀O₅

: 1424713-04-1
C₆₉H₁₃₂O₂₅

Guidance literature:: Multi-step reaction with 11 steps

1.1: tetrahydrofuran / 12 h / 65 °C

2.1: diisobutylaluminium hydride / toluene / 2 h / -78 °C / Inert atmosphere

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / toluene / -10 °C / Inert atmosphere

4.1: sodium; methanol / 1 h / 0 - 20 °C / Inert atmosphere

5.1: pyridine / 72 h / 110 °C

6.1: potassium carbonate; palladium 10% on activated carbon; hydrogen / ethyl acetate / 48 h / 20 °C / 760.05 Torr

7.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

8.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 0 °C / Inert atmosphere

8.2: 0 - 20 °C / Inert atmosphere

9.1: acetic acid / methanol / 48 h / 20 °C

10.1: water; sodium hydroxide; tetra-(n-butyl)ammonium iodide / toluene / 48 h / 45 °C

10.2: 1 h / 0 °C / Inert atmosphere

10.3: 12 h / 0 - 20 °C / Inert atmosphere

11.1: water; osmium(VIII) oxide; 4-methylmorpholine N-oxide / acetone; tert-butyl alcohol / 24 h / 0 - 20 °C

With pyridine; methanol; osmium(VIII) oxide; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; palladium 10% on activated carbon; water; hydrogen; sodium; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride; potassium carbonate; acetic acid; 4-methylmorpholine N-oxide; triphenylphosphine; sodium hydroxide; In tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene; mineral oil; tert-butyl alcohol; 3.1: |Mitsunobu Displacement / 8.2: |Williamson Ether Synthesis / 10.3: |Williamson Ether Synthesis;
DOI:10.1055/s-0032-1317929