4,4',4''-[(2,4,6-trimethylbenzene-1,3,5-triyl)tris[methylene(methylimino)methylene]]tris[2-(methoxymethoxy)benzoic acid] trimethyl ester

Base Information

Chemical Name:4,4',4''-[(2,4,6-trimethylbenzene-1,3,5-triyl)tris[methylene(methylimino)methylene]]tris[2-(methoxymethoxy)benzoic acid] trimethyl ester
CAS No.:204766-11-0
Molecular Formula:C₄₈H₆₃N₃O₁₂
Molecular Weight:874.041
Hs Code.:

Synonyms:4,4',4''-[(2,4,6-trimethylbenzene-1,3,5-triyl)tris[methylene(methylimino)methylene]]tris[2-(methoxymethoxy)benzoic acid] trimethyl ester

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Chemical Property of 4,4',4''-[(2,4,6-trimethylbenzene-1,3,5-triyl)tris[methylene(methylimino)methylene]]tris[2-(methoxymethoxy)benzoic acid] trimethyl ester

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Technology Process of 4,4',4''-[(2,4,6-trimethylbenzene-1,3,5-triyl)tris[methylene(methylimino)methylene]]tris[2-(methoxymethoxy)benzoic acid] trimethyl ester

There total 3 articles about 4,4',4''-[(2,4,6-trimethylbenzene-1,3,5-triyl)tris[methylene(methylimino)methylene]]tris[2-(methoxymethoxy)benzoic acid] trimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 149543-77-1
methyl 4-bromomethyl-2-methoxymethoxybenzoate

: 204766-10-9
Methyl-(2,4,6-trimethyl-3,5-bis-methylaminomethyl-benzyl)-amine

: 204766-11-0
4,4',4''-[(2,4,6-trimethylbenzene-1,3,5-triyl)tris[methylene(methylimino)methylene]]tris[2-(methoxymethoxy)benzoic acid] trimethyl ester

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 24h; Ambient temperature;
DOI:10.1002/hlca.19980810203

Reference yield:

: 149525-64-4
1,3,5-tris(aminomethyl)-2,4,6-trimethylbenzene

: 204766-11-0
4,4',4''-[(2,4,6-trimethylbenzene-1,3,5-triyl)tris[methylene(methylimino)methylene]]tris[2-(methoxymethoxy)benzoic acid] trimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Et₃N / CH₂Cl₂ / Ambient temperature

2: LiAlH₄ / tetrahydrofuran / Heating

3: 81 percent / K₂CO₃ / dimethylformamide / 24 h / Ambient temperature

With lithium aluminium tetrahydride; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19980810203

Reference yield:

: [3,5-Bis-(ethoxycarbonylamino-methyl)-2,4,6-trimethyl-benzyl]-carbamic acid ethyl ester

: 204766-11-0
4,4',4''-[(2,4,6-trimethylbenzene-1,3,5-triyl)tris[methylene(methylimino)methylene]]tris[2-(methoxymethoxy)benzoic acid] trimethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran / Heating

2: 81 percent / K₂CO₃ / dimethylformamide / 24 h / Ambient temperature

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19980810203