(E)-3-[3-[(E)-3-(3-Methoxy-4-methoxymethoxy-phenyl)-allyloxy]-4-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone

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Chemical Name:(E)-3-[3-[(E)-3-(3-Methoxy-4-methoxymethoxy-phenyl)-allyloxy]-4-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone
CAS No.:110450-73-2
Molecular Formula:C₃₉H₅₂O₁₃Si
Molecular Weight:756.92
Hs Code.:

(E)-3-[3-[(E)-3-(3-Methoxy-4-methoxymethoxy-phenyl)-allyloxy]-4-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone

Synonyms:(E)-3-[3-[(E)-3-(3-Methoxy-4-methoxymethoxy-phenyl)-allyloxy]-4-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone

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Chemical Property of (E)-3-[3-[(E)-3-(3-Methoxy-4-methoxymethoxy-phenyl)-allyloxy]-4-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone

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Technology Process of (E)-3-[3-[(E)-3-(3-Methoxy-4-methoxymethoxy-phenyl)-allyloxy]-4-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone

There total 5 articles about (E)-3-[3-[(E)-3-(3-Methoxy-4-methoxymethoxy-phenyl)-allyloxy]-4-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 36804-11-2
2,4,6-tri-MOM phloracetophenone

: 110450-66-3
3-[(E)-3-(3-Methoxy-4-methoxymethoxy-phenyl)-allyloxy]-4-(2-trimethylsilanyl-ethoxymethoxy)-benzaldehyde

: 110450-73-2
(E)-3-[3-[(E)-3-(3-Methoxy-4-methoxymethoxy-phenyl)-allyloxy]-4-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone

Guidance literature:: With N-benzyl-trimethylammonium hydroxide; In benzene; for 24h; Ambient temperature;
DOI:10.1246/cl.1986.2097

Reference yield:

: 110450-65-2
(E)-3-[3-methoxy-4-(methoxymethoxy)phenyl]prop-2-en-1-ol

: 110450-73-2
(E)-3-[3-[(E)-3-(3-Methoxy-4-methoxymethoxy-phenyl)-allyloxy]-4-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / Ph₃P, diethyl azodicarboxylate / tetrahydrofuran / 24 h / Ambient temperature

2: 84 percent / Triton B / benzene / 24 h / Ambient temperature

With N-benzyl-trimethylammonium hydroxide; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; benzene;
DOI:10.1246/cl.1986.2097

Reference yield:

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 110450-73-2
(E)-3-[3-[(E)-3-(3-Methoxy-4-methoxymethoxy-phenyl)-allyloxy]-4-(2-trimethylsilanyl-ethoxymethoxy)-phenyl]-1-(2,4,6-tris-methoxymethoxy-phenyl)-propenone

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / i-Pr₂NEt / CH₂Cl₂ / 3.7 h / Ambient temperature

2: 55 percent / Ph₃P, diethyl azodicarboxylate / tetrahydrofuran / 24 h / Ambient temperature

3: 84 percent / Triton B / benzene / 24 h / Ambient temperature

With N-benzyl-trimethylammonium hydroxide; N-ethyl-N,N-diisopropylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; benzene;
DOI:10.1246/cl.1986.2097