(2S,3S,4S,7S,9S)-9-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2-ethyl-3-[(4-methoxybenzyl)oxy]-4-methyl-7,9-di[(1,1,1-triisopropylsilyl)oxy]decan-1-ol

Base Information

• Chemical Name: (2S,3S,4S,7S,9S)-9-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2-ethyl-3-[(4-methoxybenzyl)oxy]-4-methyl-7,9-di[(1,1,1-triisopropylsilyl)oxy]decan-1-ol
• CAS No.: 1009089-99-9
• Molecular Formula: C₄₅H₉₀O₆Si₃
• Molecular Weight: 811.462

Synonyms:(2S,3S,4S,7S,9S)-9-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2-ethyl-3-[(4-methoxybenzyl)oxy]-4-methyl-7,9-di[(1,1,1-triisopropylsilyl)oxy]decan-1-ol

Chemical Property of (2S,3S,4S,7S,9S)-9-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2-ethyl-3-[(4-methoxybenzyl)oxy]-4-methyl-7,9-di[(1,1,1-triisopropylsilyl)oxy]decan-1-ol

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Technology Process of (2S,3S,4S,7S,9S)-9-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2-ethyl-3-[(4-methoxybenzyl)oxy]-4-methyl-7,9-di[(1,1,1-triisopropylsilyl)oxy]decan-1-ol

There total 1 articles about (2S,3S,4S,7S,9S)-9-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2-ethyl-3-[(4-methoxybenzyl)oxy]-4-methyl-7,9-di[(1,1,1-triisopropylsilyl)oxy]decan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

tert-butyl((2S,4S,7S)-6-[(4S,5S)-5-ethyl-2-(4-methoxyphenyl)-1,3-dioxan-4-yl]-2,4-di[(1,1,1-triisopropylsilyl)oxy]octyloxy)dimethylsilane (1009089-88-6) → (2S,3S,4S,7S,9S)-9-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2-ethyl-3-[(4-methoxybenzyl)oxy]-4-methyl-7,9-di[(1,1,1-triisopropylsilyl)oxy]decan-1-ol (1009089-99-9)

Guidance literature:

With diisobutylaluminium hydride; In dichloromethane; at -40 - 0 ℃; for 2.5h;

DOI:10.1021/jo7023152

Reference yield:

(2S,3S,4S,7S,9S)-9-[1-(tert-butyl)-1,1-dimethylsilyl]oxy-2-ethyl-3-[(4-methoxybenzyl)oxy]-4-methyl-7,9-di[(1,1,1-triisopropylsilyl)oxy]decan-1-ol (1009089-99-9) → C45H88O6Si3

Guidance literature:

With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1021/jo7023152

upstream raw materials:

tert-butyl((2S,4S,7S)-6-[(4S,5S)-5-ethyl-2-(4-methoxyphenyl)-1,3-dioxan-4-yl]-2,4-di[(1,1,1-triisopropylsilyl)oxy]octyloxy)dimethylsilane

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