4,6-di-O-benzyl-2,3-dideoxy-3-diethoxyphosphoryl-D-xylo-hexono-1,5-lactone

Base Information

Chemical Name:4,6-di-O-benzyl-2,3-dideoxy-3-diethoxyphosphoryl-D-xylo-hexono-1,5-lactone
CAS No.:1417781-74-8
Molecular Formula:C₂₄H₃₁O₇P
Molecular Weight:462.48
Hs Code.:

Synonyms:4,6-di-O-benzyl-2,3-dideoxy-3-diethoxyphosphoryl-D-xylo-hexono-1,5-lactone

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Chemical Property of 4,6-di-O-benzyl-2,3-dideoxy-3-diethoxyphosphoryl-D-xylo-hexono-1,5-lactone

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Technology Process of 4,6-di-O-benzyl-2,3-dideoxy-3-diethoxyphosphoryl-D-xylo-hexono-1,5-lactone

There total 1 articles about 4,6-di-O-benzyl-2,3-dideoxy-3-diethoxyphosphoryl-D-xylo-hexono-1,5-lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 131771-65-8
4,6-di-O-benzyl-2,3-dideoxy-D-threo-hex-2-enono-1,5-lactone

: 122-52-1
triethyl phosphite

: 1417781-74-8
4,6-di-O-benzyl-2,3-dideoxy-3-diethoxyphosphoryl-D-xylo-hexono-1,5-lactone

: 1417781-91-9
4,6-di-O-benzyl-2,3-dideoxy-3-diethoxyphosphoryl-D-lyxo-hexono-1,5-lactone

Guidance literature:: With phenol; at 100 ℃; for 1.5h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol302939z

Reference yield:

: 1417781-74-8
4,6-di-O-benzyl-2,3-dideoxy-3-diethoxyphosphoryl-D-xylo-hexono-1,5-lactone

: 1417781-75-9
4,6-di-O-benzyl-2,3-dideoxy-3-diethoxyphosphoryl-D-xylo-hexopyranose

: 1417781-98-6
4,6-di-O-benzyl-2,3-dideoxy-3-diethoxyphosphoryl-D-xylo-hexopyranose

Guidance literature:: 4,6-di-O-benzyl-2,3-dideoxy-3-diethoxyphosphoryl-D-xylo-hexono-1,5-lactone; With diisobutylaluminium hydride; In toluene; at -78 ℃; for 1.5h; Inert atmosphere;

In ethanol; toluene; at -78 - 0 ℃; Overall yield = 77 %; Overall yield = 78.5 mg; Inert atmosphere;
DOI:10.1021/ol302939z