diethyl <4-hydroxy-3-butyl>phosphonateyl

Base Information

Chemical Name:diethyl <4-hydroxy-3-butyl>phosphonateyl
CAS No.:134361-28-7
Molecular Formula:C₂₉H₃₇O₆P
Molecular Weight:512.583
Hs Code.:

diethyl <4-hydroxy-3-<diphenyl(4-methoxyphenyl)methoxy>butyl>phosphonateyl

Synonyms:diethyl <4-hydroxy-3-butyl>phosphonateyl

Suppliers and Price of diethyl <4-hydroxy-3-butyl>phosphonateyl

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of diethyl <4-hydroxy-3-butyl>phosphonateyl

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of diethyl <4-hydroxy-3-butyl>phosphonateyl

There total 4 articles about diethyl <4-hydroxy-3-butyl>phosphonateyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 133866-77-0
diethyl <4-hydroxy-3-(hydroxymethyl)butyl>phosphonate

: 14470-28-1
mono-4-methoxytrityl chloride

: 134361-28-7
diethyl <4-hydroxy-3-butyl>phosphonateyl

Guidance literature:: With pyridine; dmap; TEA; at 60 ℃; for 2h;
DOI:10.1021/jm00111a052

Reference yield:

: 97845-58-4
5-(2-bromoethyl)-2,2-dimethyl-1,3-dioxane

: 134361-28-7
diethyl <4-hydroxy-3-butyl>phosphonateyl

Guidance literature:: Multi-step reaction with 4 steps

1: sodium iodide / acetone / 16 h / 25 °C

2: 0.67 h / 140 °C

3: 2 N HCl / acetone / 1 h / 25 °C

4: 30 percent / pyridine, TEA, 4-(dimethylamino)pyridine / 2 h / 60 °C

With pyridine; hydrogenchloride; dmap; TEA; sodium iodide; In acetone;
DOI:10.1021/jm00111a052

Reference yield:

: 2-(2,2-dimethyl-1,3-dioxan-5-yl)ethyl iodide

: 134361-28-7
diethyl <4-hydroxy-3-butyl>phosphonateyl

Guidance literature:: Multi-step reaction with 3 steps

1: 0.67 h / 140 °C

2: 2 N HCl / acetone / 1 h / 25 °C

3: 30 percent / pyridine, TEA, 4-(dimethylamino)pyridine / 2 h / 60 °C

With pyridine; hydrogenchloride; dmap; TEA; In acetone;
DOI:10.1021/jm00111a052