2-(tert-butoxycarbonyl)-7-(phenylsulfonyl)-1,2,3,6-tetrahydroazocino[4,3-b]indole

Base Information

Chemical Name:2-(tert-butoxycarbonyl)-7-(phenylsulfonyl)-1,2,3,6-tetrahydroazocino[4,3-b]indole
CAS No.:752212-14-9
Molecular Formula:C₂₄H₂₆N₂O₄S
Molecular Weight:438.547
Hs Code.:

Synonyms:2-(tert-butoxycarbonyl)-7-(phenylsulfonyl)-1,2,3,6-tetrahydroazocino[4,3-b]indole

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Chemical Property of 2-(tert-butoxycarbonyl)-7-(phenylsulfonyl)-1,2,3,6-tetrahydroazocino[4,3-b]indole

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Technology Process of 2-(tert-butoxycarbonyl)-7-(phenylsulfonyl)-1,2,3,6-tetrahydroazocino[4,3-b]indole

There total 1 articles about 2-(tert-butoxycarbonyl)-7-(phenylsulfonyl)-1,2,3,6-tetrahydroazocino[4,3-b]indole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 752212-12-7
2-allyl-3-[(N-allyl-N-tert-butoxycarbonylamino)-methyl]-1-(phenylsulfonyl)indole

: 752212-14-9
2-(tert-butoxycarbonyl)-7-(phenylsulfonyl)-1,2,3,6-tetrahydroazocino[4,3-b]indole

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; for 2h; Reflux; Inert atmosphere;
DOI:10.1016/j.tet.2013.01.064

Reference yield: 35.0%

: 752212-14-9
2-(tert-butoxycarbonyl)-7-(phenylsulfonyl)-1,2,3,6-tetrahydroazocino[4,3-b]indole

: 1192689-94-3
2-(tert-butoxycarbonyl)-7-(phenylsulfonyl)-1,2,5,6-tetrahydro-7H-azocino[4,3-b]indole

: 1192689-96-5
2-(tert-butoxycarbonyl)-7-(phenylsulfonyl)-1,2,3,4-tetrahydro-7H-azocino[4,3-b]indole

Guidance literature:: With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In toluene; for 24h; Reflux; Inert atmosphere;
DOI:10.1021/jo901986v

Reference yield:

: 752212-14-9
2-(tert-butoxycarbonyl)-7-(phenylsulfonyl)-1,2,3,6-tetrahydroazocino[4,3-b]indole

: C₁₉H₁₈N₂O₂S

Guidance literature:: 2-(tert-butoxycarbonyl)-7-(phenylsulfonyl)-1,2,3,6-tetrahydroazocino[4,3-b]indole; With hydrogenchloride; In methanol; at 20 ℃; for 18h; Inert atmosphere;

With ammonium hydroxide; In methanol;
DOI:10.1016/j.tet.2013.01.064