phenyl 6-O-(2-naphthylmethyl)-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:phenyl 6-O-(2-naphthylmethyl)-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside
CAS No.:260411-26-5
Molecular Formula:C₃₁H₂₇NO₆S
Molecular Weight:541.624
Hs Code.:

Synonyms:phenyl 6-O-(2-naphthylmethyl)-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl 6-O-(2-naphthylmethyl)-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

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Technology Process of phenyl 6-O-(2-naphthylmethyl)-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

There total 1 articles about phenyl 6-O-(2-naphthylmethyl)-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 136882-36-5,79528-50-0
2-((2S,3R,4R,5S,6R)-4,5-Dihydroxy-6-hydroxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl)-isoindole-1,3-dione

: 939-26-4
2-bromomethylnaphthyl bromide

: 260411-26-5
phenyl 6-O-(2-naphthylmethyl)-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: 2-((2S,3R,4R,5S,6R)-4,5-Dihydroxy-6-hydroxymethyl-2-phenylsulfanyl-tetrahydro-pyran-3-yl)-isoindole-1,3-dione; With (n-Bu₃)2O; In benzene; for 4h; reflux;

2-bromomethylnaphthyl bromide; With tetrabutylammomium bromide; In benzene; at 80 - 85 ℃; for 48h;
DOI:10.1016/S0040-4039(00)00261-6

Reference yield: 87.0%

: 260411-26-5
phenyl 6-O-(2-naphthylmethyl)-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 329783-81-5
[Methyl (N-acetyl-5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosyl)onate]-(2->3)-6-O-pivaloyl-2,4-di-O-acetyl-β-D-galactopyranosyl trichloroacetimidate

: 329783-76-8
Phenyl [methyl (N-acetyl-5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-nonulopyranosyl)onate]-(2->3)-(6-O-pivaloyl-2,4-di-O-acetyl-β-D-galactopyranosyl)-(1->4)-2-deoxy-6-O-naphthylmethyl-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at -45 - -40 ℃; for 1.5h;
DOI:10.1002/1521-3765(20010119)7:2<356::AID-CHEM356>3.0.CO;2-E

Reference yield: 75.0%

: 260411-26-5
phenyl 6-O-(2-naphthylmethyl)-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

: 4163-45-5
2,3,4,6-tetra-O-acetyl-β-galactopyranosyl fluoride

: 282713-88-6
Phenyl (2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl-(1->4)-6-O-naphthylmethyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; tin(ll) chloride; In dichloromethane; toluene; at -15 - 0 ℃; for 12h;
DOI:10.1016/S0040-4039(00)00261-6