4-deuterio-2,6-diphenylthiopyran

Base Information

Chemical Name:4-deuterio-2,6-diphenylthiopyran
CAS No.:80160-63-0
Molecular Formula:C₁₇H₁₄S
Molecular Weight:251.356
Hs Code.:

Synonyms:4-deuterio-2,6-diphenylthiopyran

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Chemical Property of 4-deuterio-2,6-diphenylthiopyran

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Technology Process of 4-deuterio-2,6-diphenylthiopyran

There total 3 articles about 4-deuterio-2,6-diphenylthiopyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 13586-29-3
2,6-diphenylthiopyrilium perchlorate

: 80160-63-0
4-deuterio-2,6-diphenylthiopyran

Guidance literature:: With sodium borodeuteride; In isopropyl alcohol; for 2h; Ambient temperature;
DOI:10.1021/jo00343a015

Reference yield:

: 55221-37-9
2,6-diphenyl-4-hydroxy-4H-tetrahydrothiopyran

: 80160-63-0
4-deuterio-2,6-diphenylthiopyran

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / N-chlorosuccinimide, 4 A molecular sieves / CH₂Cl₂ / Ambient temperature

2: 1.) n-BuLi, 2.) methanol-d / 1.) THF, hexane, -77 deg C, 1 h

With N-chloro-succinimide; n-butyllithium; deuteromethanol; 4 A molecular sieve; In dichloromethane;
DOI:10.1021/jo00343a015

Reference yield:

: 71750-06-6
2,6-diphenyl-2H-thiopyran

: 80160-63-0
4-deuterio-2,6-diphenylthiopyran

Guidance literature:: With n-butyllithium; deuteromethanol; Yield given. Multistep reaction; 1.) THF, hexane, -77 deg C, 1 h;
DOI:10.1021/jo00343a015