1-deamino-2-deoxy-1-epi-hydroxystreptamine

Base Information

Chemical Name:1-deamino-2-deoxy-1-epi-hydroxystreptamine
CAS No.:22389-04-4
Molecular Formula:C₆H₁₃NO₄
Molecular Weight:163.174
Hs Code.:

Synonyms:1-deamino-2-deoxy-1-epi-hydroxystreptamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-deamino-2-deoxy-1-epi-hydroxystreptamine

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Technology Process of 1-deamino-2-deoxy-1-epi-hydroxystreptamine

There total 14 articles about 1-deamino-2-deoxy-1-epi-hydroxystreptamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 66065-95-0,66101-45-9
1-deamino-1-epi-hydroxysisomicin

: 22389-04-4,72075-06-0
1-deamino-2-deoxy-1-epi-hydroxystreptamine

Guidance literature:: With hydrogenchloride; for 18h; Heating;
DOI:10.1039/P19810002168

Reference yield:

: 140390-53-0
(1R,2R,3R,4S,5R)-5-Benzyloxyamino-cyclohexane-1,2,3,4-tetraol

: 22389-04-4,72075-06-0
1-deamino-2-deoxy-1-epi-hydroxystreptamine

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 12h; under 760 Torr; Ambient temperature;
DOI:10.1021/jo00035a017

Reference yield:

: 6207-30-3,72536-03-9
2,3:4,5-di-O-isopropylidene-D-glucose diethyl dithioacetal

: 22389-04-4,72075-06-0
1-deamino-2-deoxy-1-epi-hydroxystreptamine

Guidance literature:: Multi-step reaction with 6 steps

1: 70 percent / CBr₄/PPh₃

2: 80 percent / HgO/HgCl / acetone; H₂O / 60 °C

3: 76 percent / pyridine / CH₂Cl₂; H₂O / 18 h / Heating

4: 75 percent / tributyltin hydride, azoisobutyronitrile (AIBN) / toluene / 7 h / Heating

5: 70 percent / acetic acid / H₂O / 24 h / Ambient temperature

6: hydrogen / Pd/C (10percent) / methanol / 12 h / 760 Torr / Ambient temperature

With pyridine; 2,2'-azobis(isobutyronitrile); carbon tetrabromide; hydrogen; tri-n-butyl-tin hydride; acetic acid; triphenylphosphine; mercury(II) oxide; mercury(II) chloride; palladium on activated charcoal; In methanol; dichloromethane; water; acetone; toluene;
DOI:10.1021/jo00035a017