Technology Process of C24H36ClN5O4
There total 9 articles about C24H36ClN5O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
acetic acid; zinc;
In
ethanol;
for 1.5h;
Heating;
DOI:10.1248/cpb.38.2719
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 100 percent / pyridine / 1 h / Ambient temperature
2: 89 percent / H2 / Pd black / ethanol / 60 °C
3: 81 percent / CrO3, pyridine / Ambient temperature
4: 94 percent / NH2OH*HCl, pyridine / 1.5 h / 35 °C
5: 74 percent / H2 / PtO2 / ethanol / Ambient temperature
6: 78 percent / NEt3 / butan-1-ol / Heating
7: 67 percent / NaNO2, conc. HCl, NaOAc*3H2O / 24 h / Ambient temperature
8: 77 percent / Zn, AcOH / aq. ethanol / 1.5 h / Heating
With
pyridine; chromium(VI) oxide; hydrogenchloride; hydroxylamine hydrochloride; hydrogen; sodium acetate; acetic acid; triethylamine; zinc; sodium nitrite;
platinum(IV) oxide; palladium;
In
ethanol; butan-1-ol;
DOI:10.1248/cpb.38.2719
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 81 percent / CrO3, pyridine / Ambient temperature
2: 94 percent / NH2OH*HCl, pyridine / 1.5 h / 35 °C
3: 74 percent / H2 / PtO2 / ethanol / Ambient temperature
4: 78 percent / NEt3 / butan-1-ol / Heating
5: 67 percent / NaNO2, conc. HCl, NaOAc*3H2O / 24 h / Ambient temperature
6: 77 percent / Zn, AcOH / aq. ethanol / 1.5 h / Heating
With
pyridine; chromium(VI) oxide; hydrogenchloride; hydroxylamine hydrochloride; hydrogen; sodium acetate; acetic acid; triethylamine; zinc; sodium nitrite;
platinum(IV) oxide;
In
ethanol; butan-1-ol;
DOI:10.1248/cpb.38.2719
