C₂₀H₂₄BrNO₃S

Base Information

Chemical Name:C₂₀H₂₄BrNO₃S
CAS No.:1392015-32-5
Molecular Formula:C₂₀H₂₄BrNO₃S
Molecular Weight:438.385
Hs Code.:

C<sub>20</sub>H<sub>24</sub>BrNO<sub>3</sub>S

Synonyms:C₂₀H₂₄BrNO₃S

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Chemical Property of C₂₀H₂₄BrNO₃S

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Technology Process of C₂₀H₂₄BrNO₃S

There total 1 articles about C₂₀H₂₄BrNO₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 79-20-9
acetic acid methyl ester

: 1392015-31-4
(R)-N-[(3-bromophenyl)(phenyl)methylene]-2-methylpropane-2-sulfinamide

: 1392015-32-5
C₂₀H₂₄BrNO₃S

Guidance literature:: acetic acid methyl ester; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

(R)-N-[(3-bromophenyl)(phenyl)methylene]-2-methylpropane-2-sulfinamide; With chlorotitanium triisopropoxide; In tetrahydrofuran; hexane; at -78 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ml3001165

Reference yield:

: 1392015-32-5
C₂₀H₂₄BrNO₃S

: C₁₆H₁₆BrNO₂

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; 1,4-dioxane; methanol; at 20 ℃; for 1.5h;
DOI:10.1021/ml3001165

Reference yield:

: 1392015-32-5
C₂₀H₂₄BrNO₃S

: 1392015-34-7
C₂₉H₃₁N₃O₄

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / tetrahydrofuran; 1,4-dioxane; methanol / 1.5 h / 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / tetrahydrofuran; N,N-dimethyl-formamide / 50 °C

3: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate / dichloromethane; tert-butyl alcohol / 1.5 h / 60 °C

With hydrogenchloride; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1021/ml3001165