acide (hydroxy-α methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylique

Base Information

• Chemical Name: acide (hydroxy-α methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylique
• CAS No.: 104225-53-8
• Molecular Formula: C₁₇H₂₄O₄
• Molecular Weight: 292.375

Synonyms:acide (hydroxy-α methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylique

Chemical Property of acide (hydroxy-α methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylique

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Technology Process of acide (hydroxy-α methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylique

There total 3 articles about acide (hydroxy-α methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylique which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

acide (-)-cis-p-anisoyl-3 trimethyl-1,2,2 cyclopentane carboxylique (145415-55-0,82801-37-4) → acide (hydroxy-α methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylique (104225-53-8)

Guidance literature:

With sodium tetrahydroborate; sodium carbonate; In methanol; water; at 18 - 25 ℃;

Reference yield: 9.0%

acide (-)-cis-p-anisoyl-3 trimethyl-1,2,2 cyclopentane carboxylique (145415-55-0,82801-37-4) → (hydroxy-α' methoxy-4' benzyl)-3 hydroxy methyl-1 trimethyl-1,2,2 cyclopentane (104225-57-2) + acide (hydroxy-α methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylique (104225-53-8)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 1h; Heating;

Reference yield:

acide (-)-trans-p-anisoyl-3 trimethyl-1,2,2 cyclopentane carboxylique (145415-56-1,82801-37-4) → acide (methoxy-4 benzylidene)-3 trimethyl-1,2,2 cyclopentane carboxylique (104225-54-9) + acide (hydroxy-α methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carboxylique trans (104225-53-8)

Guidance literature:

With sodium tetrahydroborate; sodium carbonate; In methanol; water; at 18 - 25 ℃;

upstream raw materials:

acide (-)-cis-p-anisoyl-3 trimethyl-1,2,2 cyclopentane carboxylique

acide (-)-trans-p-anisoyl-3 trimethyl-1,2,2 cyclopentane carboxylique

Downstream raw materials:

(methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carbolactone-1⁽³⁾

acide (methoxy-4 benzylidene)-3 trimethyl-1,2,2 cyclopentane carboxylique

(bromo-α methoxy-4 benzyl)-3 trimethyl-1,2,2 cyclopentane carbolactone-1(3)

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