(R)-3-Methanesulfinyl-2-(4-nitro-benzyloxycarbonylamino)-propionic acid allyl ester

Base Information

• Chemical Name: (R)-3-Methanesulfinyl-2-(4-nitro-benzyloxycarbonylamino)-propionic acid allyl ester
• CAS No.: 237768-94-4
• Molecular Formula: C₁₅H₁₈N₂O₇S
• Molecular Weight: 370.383
• Mol file: 237768-94-4.mol

Synonyms:(R)-3-Methanesulfinyl-2-(4-nitro-benzyloxycarbonylamino)-propionic acid allyl ester

Chemical Property of (R)-3-Methanesulfinyl-2-(4-nitro-benzyloxycarbonylamino)-propionic acid allyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (R)-3-Methanesulfinyl-2-(4-nitro-benzyloxycarbonylamino)-propionic acid allyl ester

There total 1 articles about (R)-3-Methanesulfinyl-2-(4-nitro-benzyloxycarbonylamino)-propionic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(R)-3-Methylsulfanyl-2-(4-nitro-benzyloxycarbonylamino)-propionic acid allyl ester → (R)-3-Methanesulfinyl-2-(4-nitro-benzyloxycarbonylamino)-propionic acid allyl ester (237768-94-4)

Guidance literature:

With sodium periodate; In methanol; water; at 25 ℃; for 7h;

DOI:10.1021/ja990851a

Reference yield:

(R)-3-Methanesulfinyl-2-(4-nitro-benzyloxycarbonylamino)-propionic acid allyl ester (237768-94-4) → C15H19N3O7S (237768-95-5)

Guidance literature:

With mesitylenesulfonylhydroxylamine; In acetonitrile; at 25 ℃; for 72h; Yield given;

DOI:10.1021/ja990851a

Reference yield:

(R)-3-Methanesulfinyl-2-(4-nitro-benzyloxycarbonylamino)-propionic acid allyl ester (237768-94-4) → C31H39N8O12PS

Guidance literature:

Multi-step reaction with 2 steps

1: O-mesitylsulfonylhydroxylamine / acetonitrile / 72 h / 25 °C

2: 1H-tetrazole / acetonitrile / 4 h / 25 °C

With 1H-tetrazole; mesitylenesulfonylhydroxylamine; In acetonitrile;

DOI:10.1021/ja990851a

Downstream raw materials:

C₁₅H₁₉N₃O₇S

C₃₁H₃₉N₈O₁₃PS