2-(4-methyl-5-thiophen-2-yl-4H-[1,2,4]triazol-3-ylsulfanyl)-propionic acid

Base Information

Chemical Name:2-(4-methyl-5-thiophen-2-yl-4H-[1,2,4]triazol-3-ylsulfanyl)-propionic acid
CAS No.:660417-64-1
Molecular Formula:C₁₀H₁₁N₃O₂S₂
Molecular Weight:269.348
Hs Code.:

Synonyms:2-(4-methyl-5-thiophen-2-yl-4H-[1,2,4]triazol-3-ylsulfanyl)-propionic acid

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Chemical Property of 2-(4-methyl-5-thiophen-2-yl-4H-[1,2,4]triazol-3-ylsulfanyl)-propionic acid

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Technology Process of 2-(4-methyl-5-thiophen-2-yl-4H-[1,2,4]triazol-3-ylsulfanyl)-propionic acid

There total 1 articles about 2-(4-methyl-5-thiophen-2-yl-4H-[1,2,4]triazol-3-ylsulfanyl)-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 12.0%

: 68744-66-1
4-methyl-5-(thiophen-2-yl)-4H-1,2,4-triazole-3-thiol

: 7474-05-7
(R)-2-chloropropionic acid

: 660417-64-1
2-(4-methyl-5-thiophen-2-yl-4H-[1,2,4]triazol-3-ylsulfanyl)-propionic acid

Guidance literature:: 4-methyl-5-(thiophen-2-yl)-4H-1,2,4-triazole-3-thiol; (R)-2-chloropropionic acid; With potassium carbonate; In acetonitrile; at 20 ℃; for 2.5h;

In DMF (N,N-dimethyl-formamide);

Reference yield: 66.9%

: 660417-64-1
2-(4-methyl-5-thiophen-2-yl-4H-[1,2,4]triazol-3-ylsulfanyl)-propionic acid

: 22179-77-7
3-chloro-N-hydroxy-benzamidine

: 3-(3-chloro-phenyl)-5-[1-(4-methyl-5-thiophen-2-yl-4H-[1,2,4]triazol-3-ylsulfanyl)-ethyl]-[1,2,4]oxadiazole

Guidance literature:: 2-(4-methyl-5-thiophen-2-yl-4H-[1,2,4]triazol-3-ylsulfanyl)-propionic acid; 3-chloro-N-hydroxy-benzamidine; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In DMF (N,N-dimethyl-formamide); at 20 ℃;

In DMF (N,N-dimethyl-formamide); at 135 ℃; for 3h;