C₂₄H₃₂O₅S

Base Information

Chemical Name:C₂₄H₃₂O₅S
CAS No.:948297-20-9
Molecular Formula:C₂₄H₃₂O₅S
Molecular Weight:432.581
Hs Code.:

C<sub>24</sub>H<sub>32</sub>O<sub>5</sub>S

Synonyms:C₂₄H₃₂O₅S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₄H₃₂O₅S

Chemical Property:

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Technology Process of C₂₄H₃₂O₅S

There total 8 articles about C₂₄H₃₂O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 948297-19-6
C₂₄H₃₀O₅S

: 948297-20-9
C₂₄H₃₂O₅S

Guidance literature:: With dimethylsulfide borane complex; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; at 0 - 6 ℃; for 0.333333h; optical yield given as %ee;
DOI:10.1021/ja804659n

Reference yield:

: 32400-25-2
t-butyl pent-4-enoate

: 948297-20-9
C₂₄H₃₂O₅S

Guidance literature:: Multi-step reaction with 4 steps

1.1: 88 percent / Grubbs-Hoveyda catalyst / CH₂Cl₂ / 40 °C

2.1: n-BuLi / diethyl ether / -78 °C

2.2: MgBr₂*OEt₂ / diethyl ether / -78 - 0 °C

2.3: THF / diethyl ether / 20 °C

3.1: 4-dimethylaminopyridine; pyridine / CH₂Cl₂

4.1: (S)-1-Me-3,3-diPh-tetrahydropyrrolo[1,2-c][1,3,2]oxazaborole; BH₃*SMe₂ / tetrahydrofuran / 0 °C

With pyridine; dmap; n-butyllithium; dimethylsulfide borane complex; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; [1,3-bis-(2,4,6-trimethylphenyl)-2-imidazolidinylidene]dichloro(O-isopropoxyphenylmethylene)ruthenium; In tetrahydrofuran; diethyl ether; dichloromethane; 4.1: Corey-Bakshi-Shibata reduction;
DOI:10.1002/anie.200701515

Reference yield:

: 948297-19-6
C₂₄H₃₀O₅S

: 948297-20-9
C₂₄H₃₂O₅S

: C₂₄H₃₂O₅S

Guidance literature:: With dimethylsulfide borane complex; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; at 0 ℃; Title compound not separated from byproducts.;
DOI:10.1002/anie.200701515