4-benzyloxy-N-{2-[3-(tert-butyldimethylsilyloxy)propoxy]phenyl}-3,5-dichlorobenzamide

Base Information

Chemical Name:4-benzyloxy-N-{2-[3-(tert-butyldimethylsilyloxy)propoxy]phenyl}-3,5-dichlorobenzamide
CAS No.:888731-97-3
Molecular Formula:C₂₉H₃₅Cl₂NO₄Si
Molecular Weight:560.593
Hs Code.:

Synonyms:4-benzyloxy-N-{2-[3-(tert-butyldimethylsilyloxy)propoxy]phenyl}-3,5-dichlorobenzamide

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Chemical Property of 4-benzyloxy-N-{2-[3-(tert-butyldimethylsilyloxy)propoxy]phenyl}-3,5-dichlorobenzamide

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Technology Process of 4-benzyloxy-N-{2-[3-(tert-butyldimethylsilyloxy)propoxy]phenyl}-3,5-dichlorobenzamide

There total 4 articles about 4-benzyloxy-N-{2-[3-(tert-butyldimethylsilyloxy)propoxy]phenyl}-3,5-dichlorobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 592552-29-9
2-(3-((tert-butyldimethylsilyl)oxy)propoxy)aniline

: 354575-15-8
3,5-dichloro-4-benzoxybenzoic chloride

: 888731-97-3
4-benzyloxy-N-{2-[3-(tert-butyldimethylsilyloxy)propoxy]phenyl}-3,5-dichlorobenzamide

Guidance literature:: With pyridine; In chloroform; at 20 ℃; for 1h;

Reference yield:

: 888731-96-2
tert-butyldimethyl[3-(2-nitrophenoxy)propoxy]silane

: 888731-97-3
4-benzyloxy-N-{2-[3-(tert-butyldimethylsilyloxy)propoxy]phenyl}-3,5-dichlorobenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium-carbon / tetrahydrofuran / 0 - 40 °C

2: pyridine / chloroform / 1 h / 0 - 40 °C

With pyridine; hydrogen; palladium-carbon; In tetrahydrofuran; chloroform;

Reference yield:

: 89031-84-5
3-(tert-butyldimethylsilyloxy)propyl bromide

: 888731-97-3
4-benzyloxy-N-{2-[3-(tert-butyldimethylsilyloxy)propoxy]phenyl}-3,5-dichlorobenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 - 40 °C

1.2: 40 - 90 °C

2.1: hydrogen / palladium-carbon / tetrahydrofuran / 0 - 40 °C

3.1: pyridine / chloroform / 1 h / 0 - 40 °C

With pyridine; hydrogen; sodium hydride; palladium-carbon; In tetrahydrofuran; chloroform; N,N-dimethyl-formamide;