1-({2-benzyl-2-[(3-hydroxy-2,2-dimethyl-1-oxopropyl)amino]-1-oxopropyl}amino)-N,N-dimethylcyclopentanecarboxamide

Base Information

Chemical Name:1-({2-benzyl-2-[(3-hydroxy-2,2-dimethyl-1-oxopropyl)amino]-1-oxopropyl}amino)-N,N-dimethylcyclopentanecarboxamide
CAS No.:266338-74-3
Molecular Formula:C₂₃H₃₅N₃O₄
Molecular Weight:417.549
Hs Code.:

Synonyms:1-({2-benzyl-2-[(3-hydroxy-2,2-dimethyl-1-oxopropyl)amino]-1-oxopropyl}amino)-N,N-dimethylcyclopentanecarboxamide

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Chemical Property of 1-({2-benzyl-2-[(3-hydroxy-2,2-dimethyl-1-oxopropyl)amino]-1-oxopropyl}amino)-N,N-dimethylcyclopentanecarboxamide

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Technology Process of 1-({2-benzyl-2-[(3-hydroxy-2,2-dimethyl-1-oxopropyl)amino]-1-oxopropyl}amino)-N,N-dimethylcyclopentanecarboxamide

There total 4 articles about 1-({2-benzyl-2-[(3-hydroxy-2,2-dimethyl-1-oxopropyl)amino]-1-oxopropyl}amino)-N,N-dimethylcyclopentanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 108805-12-5
3'-(Dimethylamino)spiroazirin>

: 266338-70-9
2-benzyl-2-[(3-hydroxy-2,2-dimethyl-1-oxopropyl)amino]propanoic acid

: 266338-74-3
1-({2-benzyl-2-[(3-hydroxy-2,2-dimethyl-1-oxopropyl)amino]-1-oxopropyl}amino)-N,N-dimethylcyclopentanecarboxamide

Guidance literature:: In acetonitrile; at 20 ℃; for 25h;
DOI:10.1002/(SICI)1522-2675(20000119)83:1<233::AID-HLCA233>3.0.CO;2-1

Reference yield:

: 4835-90-9
3-Hydroxy-2,2-dimethylpropanoic acid

: 266338-74-3
1-({2-benzyl-2-[(3-hydroxy-2,2-dimethyl-1-oxopropyl)amino]-1-oxopropyl}amino)-N,N-dimethylcyclopentanecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / acetonitrile / 30 h / 20 °C

2: 95 percent / aq. HCl / tetrahydrofuran / 26 h / 20 °C

3: 92 percent / acetonitrile / 25 h / 20 °C

With hydrogenchloride; In tetrahydrofuran; acetonitrile; 1: Addition / 2: Hydrolysis / 3: Addition;
DOI:10.1002/(SICI)1522-2675(20000119)83:1<233::AID-HLCA233>3.0.CO;2-1

Reference yield:

: 114234-21-8
2-benzyl-3-(dimethylamino)-2-methyl-2H-azirine

: 266338-74-3
1-({2-benzyl-2-[(3-hydroxy-2,2-dimethyl-1-oxopropyl)amino]-1-oxopropyl}amino)-N,N-dimethylcyclopentanecarboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / acetonitrile / 30 h / 20 °C

2: 95 percent / aq. HCl / tetrahydrofuran / 26 h / 20 °C

3: 92 percent / acetonitrile / 25 h / 20 °C

With hydrogenchloride; In tetrahydrofuran; acetonitrile; 1: Addition / 2: Hydrolysis / 3: Addition;
DOI:10.1002/(SICI)1522-2675(20000119)83:1<233::AID-HLCA233>3.0.CO;2-1