Ethyl N--L-prolinate

Base Information

Chemical Name:Ethyl N--L-prolinate
CAS No.:136583-40-9
Molecular Formula:C₂₉H₃₄N₂O₄
Molecular Weight:474.6
Hs Code.:

Ethyl N-<N-Acetyl-2,2-bis(3-phenylprop-2-en-1-yl)glycyl>-L-prolinate

Synonyms:Ethyl N--L-prolinate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl N--L-prolinate

Chemical Property:

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Technology Process of Ethyl N--L-prolinate

There total 4 articles about Ethyl N--L-prolinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 108-24-7
acetic anhydride

: 136583-30-7
Ethyl N-(2-Nitro-2,2-bis(3-phenylprop-2-en-1-yl)acetyl)-L-prolinate

: 136583-40-9
Ethyl N--L-prolinate

Guidance literature:: With acetic acid; zinc; at 40 - 60 ℃;
DOI:10.1002/hlca.19910740516

Reference yield:

: 21040-45-9
Cinnamyl acetate

: 136583-40-9
Ethyl N--L-prolinate

Guidance literature:: Multi-step reaction with 3 steps

1: 1) 1,8-diazabicyclo<5.4.0>undec-7-ene, bis(dibenzylidene)palladium⁽⁰⁾, PPh₃ / 1) MeCN, 5 min; 2) MeCN, 25-30 deg C, 8-10 h

2: 1) 1,8-diazabicyclo<5.4.0>undec-7-ene, bis(dibenzylidene)palladium⁽⁰⁾, PPh₃ / 1) MeCN, 5 min; 2) MeCN, 25-30 deg C, 8-10 h

3: 60 percent / Zn, HOAc / 40 - 60 °C

With acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; zinc;
DOI:10.1002/hlca.19910740516

Reference yield:

: 129222-49-7
N-Nitroacetyl-(S)-proline ethyl ester

: 136583-40-9
Ethyl N--L-prolinate

Guidance literature:: Multi-step reaction with 3 steps

1: 1) 1,8-diazabicyclo<5.4.0>undec-7-ene, bis(dibenzylidene)palladium⁽⁰⁾, PPh₃ / 1) MeCN, 5 min; 2) MeCN, 25-30 deg C, 8-10 h

2: 1) 1,8-diazabicyclo<5.4.0>undec-7-ene, bis(dibenzylidene)palladium⁽⁰⁾, PPh₃ / 1) MeCN, 5 min; 2) MeCN, 25-30 deg C, 8-10 h

3: 60 percent / Zn, HOAc / 40 - 60 °C

With acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; zinc;
DOI:10.1002/hlca.19910740516