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Technology Process of C23H31IO3

C23H31IO3

Base Information
  • Chemical Name:C23H31IO3
  • CAS No.:1032193-36-4
  • Molecular Formula:C23H31IO3
  • Molecular Weight:482.402
  • Hs Code.:
C<sub>23</sub>H<sub>31</sub>IO<sub>3</sub>

Synonyms:C23H31IO3

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Chemical Property of C23H31IO3
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Technology Process of C23H31IO3

There total 1 articles about C23H31IO3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

C<sub>23</sub>H<sub>32</sub>O<sub>4</sub>
943858-51-3

C23H32O4

C<sub>23</sub>H<sub>31</sub>IO<sub>3</sub>
1032193-36-4

C23H31IO3

Guidance literature:
With 1H-imidazole; iodine; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 0.25h;
DOI:10.1021/jo900332q

Reference yield: 94.0%

C<sub>23</sub>H<sub>31</sub>IO<sub>3</sub>
1032193-36-4

C23H31IO3

C<sub>22</sub>H<sub>33</sub>IO<sub>5</sub>Si
1032193-52-4

C22H33IO5Si

C<sub>45</sub>H<sub>64</sub>O<sub>8</sub>Si
1032193-57-9

C45H64O8Si

Guidance literature:
C23H31IO3; With tert.-butyl lithium; 9-methoxy-9-BBN; In tetrahydrofuran; diethyl ether; hexane; at -78 - 20 ℃; for 1.08333h;
C22H33IO5Si; With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; triphenyl-arsane; caesium carbonate; In tetrahydrofuran; diethyl ether; hexane; water; N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1021/jo900332q

Reference yield: 75.0%

C<sub>23</sub>H<sub>31</sub>IO<sub>3</sub>
1032193-36-4

C23H31IO3

C<sub>22</sub>H<sub>33</sub>IO<sub>5</sub>Si

C22H33IO5Si

C<sub>45</sub>H<sub>64</sub>O<sub>8</sub>Si
1032193-37-5

C45H64O8Si

Guidance literature:
C23H31IO3; With tert.-butyl lithium; 9-methoxy-9-BBN; In tetrahydrofuran; diethyl ether; hexane; at -78 - 20 ℃; for 1.08333h;
C22H33IO5Si; With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; triphenyl-arsane; caesium carbonate; In tetrahydrofuran; diethyl ether; hexane; water; N,N-dimethyl-formamide; at 50 ℃; for 2h;
DOI:10.1021/jo900332q
upstream raw materials:

C23H32O4

Downstream raw materials:

C45H64O8Si

C45H64O8Si

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