C₁₁H₁₃ClOS

Base Information

• Chemical Name: C₁₁H₁₃ClOS
• CAS No.: 885947-60-4
• Molecular Formula: C₁₁H₁₃ClOS
• Molecular Weight: 228.743
• Mol file: 885947-60-4.mol

Synonyms:C₁₁H₁₃ClOS

Chemical Property of C₁₁H₁₃ClOS

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₁₁H₁₃ClOS

There total 2 articles about C₁₁H₁₃ClOS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

p-Chlorothiophenol (106-54-7) + 2-methyl-but-3-yn-2-ol (115-19-5) → C11H13ClOS (885947-60-4)

Guidance literature:

With (N,N′-bis(2,4,6-trimethylphenyl)imidazole-2-ylidene)Pd(acac)Cl; 3-isopropyl-6-methylcyclohexa-1,4-diene; triethylamine; In neat (no solvent); at 50 ℃; for 18h; regioselective reaction; Green chemistry;

DOI:10.1021/acscatal.5b01815

Reference yield:

p-Chlorothiophenol (106-54-7) + 2-methyl-but-3-yn-2-ol (115-19-5) → C11H13ClOS (105512-43-4) + C11H13ClOS (885947-60-4)

Guidance literature:

With aluminum oxide; potassium fluoride; potassium fluoride on basic alumina; at 60 ℃; for 3h;

DOI:10.1016/j.tetlet.2008.01.093

upstream raw materials:

p-Chlorothiophenol

2-methyl-but-3-yn-2-ol