1-Benzyl-1,4-epoxy-1,2,3,4-tetrahydro-2,3-naphthalic anhydride

Base Information

• Chemical Name: 1-Benzyl-1,4-epoxy-1,2,3,4-tetrahydro-2,3-naphthalic anhydride
• CAS No.: 73245-12-2
• Molecular Formula: C₁₉H₁₄O₄
• Molecular Weight: 306.318
• Mol file: 73245-12-2.mol

Synonyms:1-Benzyl-1,4-epoxy-1,2,3,4-tetrahydro-2,3-naphthalic anhydride

Chemical Property of 1-Benzyl-1,4-epoxy-1,2,3,4-tetrahydro-2,3-naphthalic anhydride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-Benzyl-1,4-epoxy-1,2,3,4-tetrahydro-2,3-naphthalic anhydride

There total 1 articles about 1-Benzyl-1,4-epoxy-1,2,3,4-tetrahydro-2,3-naphthalic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

maleic anhydride (108-31-6) + 1-benzyl-isobenzofuran (61200-14-4) → 1-Benzyl-1,4-epoxy-1,2,3,4-tetrahydro-2,3-naphthalic anhydride (73245-12-2) + 1-Benzyl-1,4-epoxy-1,2,3,4-tetrahydro-2,3-naphthalic anhydride (73194-90-8)

Guidance literature:

In benzene; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Heating;

DOI:10.1021/jo01298a014

Reference yield: 74.0%

1-Benzyl-1,4-epoxy-1,2,3,4-tetrahydro-2,3-naphthalic anhydride (73245-12-2) + 1-Benzyl-1,4-epoxy-1,2,3,4-tetrahydro-2,3-naphthalic anhydride (73194-90-8) → 1-Benzyl-2,3-naphthalenedicarboxylic anhydride (73194-81-7)

Guidance literature:

With chloro-trimethyl-silane; sodium iodide; In acetonitrile; for 24h; Heating;

DOI:10.1021/jo01298a014

upstream raw materials:

maleic anhydride

1-benzyl-isobenzofuran

Downstream raw materials:

1-Benzyl-2,3-naphthalenedicarboxylic anhydride