1--4,8-N-(2-mesitylenesulfonyl)-11--4,8-diazaundecane

Base Information

Chemical Name:1--4,8-N-(2-mesitylenesulfonyl)-11--4,8-diazaundecane
CAS No.:226723-96-2
Molecular Formula:C₅₅H₈₂N₄O₈S₄
Molecular Weight:1055.54
Hs Code.:

1-<N-(cycloheptymethyl)-N-(2-mesitylenesulfonyl)amino>-4,8-N-(2-mesitylenesulfonyl)-11-<N-ethyl-N-(2-mesitylenesulfonyl)amino>-4,8-diazaundecane

Synonyms:1--4,8-N-(2-mesitylenesulfonyl)-11--4,8-diazaundecane

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Chemical Property of 1--4,8-N-(2-mesitylenesulfonyl)-11--4,8-diazaundecane

Chemical Property:

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Technology Process of 1--4,8-N-(2-mesitylenesulfonyl)-11--4,8-diazaundecane

There total 3 articles about 1--4,8-N-(2-mesitylenesulfonyl)-11--4,8-diazaundecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 151915-13-8
1-<amino>-4,8-bis-11-amino-4,8-diazaundecane

: 226723-95-1
cycloheptylmethyl iodide

: 226723-96-2
1--4,8-N-(2-mesitylenesulfonyl)-11--4,8-diazaundecane

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;
DOI:10.1021/jm980603+

Reference yield:

: 4448-75-3
cycloheptylmethanol

: 226723-96-2
1--4,8-N-(2-mesitylenesulfonyl)-11--4,8-diazaundecane

Guidance literature:: Multi-step reaction with 3 steps

1: 97.9 percent / Et₃N / CH₂Cl₂ / Ambient temperature

2: 77.5 percent / NaI / acetone / 3 h / Heating

3: 84 percent / NaH / dimethylformamide / 0.5 h / 0 °C

With sodium hydride; triethylamine; sodium iodide; In dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm980603+

Reference yield:

: 75646-22-9
methane-sulphonyloxymethylcycloheptane

: 226723-96-2
1--4,8-N-(2-mesitylenesulfonyl)-11--4,8-diazaundecane

Guidance literature:: Multi-step reaction with 2 steps

1: 77.5 percent / NaI / acetone / 3 h / Heating

2: 84 percent / NaH / dimethylformamide / 0.5 h / 0 °C

With sodium hydride; sodium iodide; In N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm980603+