2-[2-(4-fluoro-phenyl)-2-oxo-1-phenyl-ethyl]-3-oxo-pentanoic acid phenylamide

Base Information

Chemical Name:2-[2-(4-fluoro-phenyl)-2-oxo-1-phenyl-ethyl]-3-oxo-pentanoic acid phenylamide
CAS No.:912998-80-2
Molecular Formula:C₂₅H₂₂FNO₃
Molecular Weight:403.453
Hs Code.:

Synonyms:2-[2-(4-fluoro-phenyl)-2-oxo-1-phenyl-ethyl]-3-oxo-pentanoic acid phenylamide

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Chemical Property of 2-[2-(4-fluoro-phenyl)-2-oxo-1-phenyl-ethyl]-3-oxo-pentanoic acid phenylamide

Chemical Property:

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Technology Process of 2-[2-(4-fluoro-phenyl)-2-oxo-1-phenyl-ethyl]-3-oxo-pentanoic acid phenylamide

There total 5 articles about 2-[2-(4-fluoro-phenyl)-2-oxo-1-phenyl-ethyl]-3-oxo-pentanoic acid phenylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 912998-79-9
2-benzylidene-3-oxo-pentanoic acid phenylamide

: 459-57-4
4-fluorobenzaldehyde

: 912998-80-2
2-[2-(4-fluoro-phenyl)-2-oxo-1-phenyl-ethyl]-3-oxo-pentanoic acid phenylamide

Guidance literature:: With 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; triethylamine; In ethanol; isopropyl alcohol; at 20 - 80 ℃; for 14h;

Reference yield:

: 62-53-3
aniline

: 912998-80-2
2-[2-(4-fluoro-phenyl)-2-oxo-1-phenyl-ethyl]-3-oxo-pentanoic acid phenylamide

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 24 h / Heating / reflux

2: acetic acid; 3-amino propanoic acid / hexanes / 28 h / Heating / reflux

3: 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; triethylamine / ethanol; isopropyl alcohol / 14 h / 20 - 80 °C

With 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; acetic acid; triethylamine; 3-amino propanoic acid; In hexanes; ethanol; isopropyl alcohol; toluene;

Reference yield:

: 30414-53-0
methyl propanoyl acetate

: 912998-80-2
2-[2-(4-fluoro-phenyl)-2-oxo-1-phenyl-ethyl]-3-oxo-pentanoic acid phenylamide

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 24 h / Heating / reflux

2: acetic acid; 3-amino propanoic acid / hexanes / 28 h / Heating / reflux

3: 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; triethylamine / ethanol; isopropyl alcohol / 14 h / 20 - 80 °C

With 3-ethyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazolium bromide; acetic acid; triethylamine; 3-amino propanoic acid; In hexanes; ethanol; isopropyl alcohol; toluene;