{(triphenylphosphine)dicarbonyl(η6-1-tri-n-butylstannylbenzene)chromium}

Base Information

Chemical Name:{(triphenylphosphine)dicarbonyl(η6-1-tri-n-butylstannylbenzene)chromium}
CAS No.:140864-42-2
Molecular Formula:C₃₈H₄₇CrO₂PSn
Molecular Weight:737.47
Hs Code.:

Synonyms:{(triphenylphosphine)dicarbonyl(η6-1-tri-n-butylstannylbenzene)chromium}

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Chemical Property of {(triphenylphosphine)dicarbonyl(η6-1-tri-n-butylstannylbenzene)chromium}

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Technology Process of {(triphenylphosphine)dicarbonyl(η6-1-tri-n-butylstannylbenzene)chromium}

There total 1 articles about {(triphenylphosphine)dicarbonyl(η6-1-tri-n-butylstannylbenzene)chromium} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 140864-41-1
{tricarbonyl(η6-1-tri-n-butylstannylbenzene)chromium}

: 140864-42-2
{(triphenylphosphine)dicarbonyl(η6-1-tri-n-butylstannylbenzene)chromium}

Guidance literature:: With triphenylphosphine; In benzene; Irradiation (UV/VIS); irradiation (175 Watt medium pressure mercury lamp) for 42 h; evapn. (vac.), column chromy. and evapn.;
DOI:10.1016/S0277-5387(00)83176-9

Reference yield: 87.0%

: 140864-42-2
{(triphenylphosphine)dicarbonyl(η6-1-tri-n-butylstannylbenzene)chromium}

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 140864-43-3
{(triphenylphosphine)dicarbonyl(η6-PPh2-benzene)chromium}

Guidance literature:: With n-butyllithium; In benzene; stirring of the Cr compd. with nBuLi in benzene at -78°C under N2 for 30 min, addn. of ClPPh2 and warming to room temp. (25 min); evapn. (vac.), column chromy. on alumina, elution with petroleum ether-ethyl acetate and evapn. (vac.); elem. anal.;
DOI:10.1016/S0277-5387(00)83176-9