n-dodecyl 2,3-di-O-dibenzyl-4,6-bis-O-[2-hydroxyethyl]-β-D-glucopyranoside

Base Information

Chemical Name:n-dodecyl 2,3-di-O-dibenzyl-4,6-bis-O-[2-hydroxyethyl]-β-D-glucopyranoside
CAS No.:1309439-34-6
Molecular Formula:C₃₆H₅₆O₈
Molecular Weight:616.836
Hs Code.:

Synonyms:n-dodecyl 2,3-di-O-dibenzyl-4,6-bis-O-[2-hydroxyethyl]-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of n-dodecyl 2,3-di-O-dibenzyl-4,6-bis-O-[2-hydroxyethyl]-β-D-glucopyranoside

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Technology Process of n-dodecyl 2,3-di-O-dibenzyl-4,6-bis-O-[2-hydroxyethyl]-β-D-glucopyranoside

There total 2 articles about n-dodecyl 2,3-di-O-dibenzyl-4,6-bis-O-[2-hydroxyethyl]-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1309439-35-7
C₄₄H₆₈O₁₀

: 1309439-34-6
n-dodecyl 2,3-di-O-dibenzyl-4,6-bis-O-[2-hydroxyethyl]-β-D-glucopyranoside

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 2h;
DOI:10.1016/j.carres.2011.03.002

Reference yield:

: 1055034-25-7
dodecyl 2,3–di–O–benzyl–β–D–glucopyranoside

: 1309439-34-6
n-dodecyl 2,3-di-O-dibenzyl-4,6-bis-O-[2-hydroxyethyl]-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / water; toluene / 0.5 h / 10 °C

1.2: 0.5 h / 10 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C

With lithium aluminium tetrahydride; tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide; In tetrahydrofuran; water; toluene;
DOI:10.1016/j.carres.2011.03.002

Reference yield: 40.0%

: 1309439-34-6
n-dodecyl 2,3-di-O-dibenzyl-4,6-bis-O-[2-hydroxyethyl]-β-D-glucopyranoside

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 1309439-36-8
n-dodecyl 2,3-O-dibenzyl-4,6-O-[19-crown-6]-β-D-glucopyranoside

Guidance literature:: n-dodecyl 2,3-di-O-dibenzyl-4,6-bis-O-[2-hydroxyethyl]-β-D-glucopyranoside; With sodium hydride; In tetrahydrofuran; paraffin oil; for 1h; Reflux;

triethylene glycol di-(p-toluenesulfonate); In tetrahydrofuran; paraffin oil; for 75h; Reflux;
DOI:10.1016/j.carres.2011.03.002