potassium 5-(4-bromobenzyloxy)pentyltrifluoride

Base Information

Chemical Name:potassium 5-(4-bromobenzyloxy)pentyltrifluoride
CAS No.:1086975-29-2
Molecular Formula:C₁₂H₁₆BBrF₃O*K
Molecular Weight:363.067
Hs Code.:

Synonyms:potassium 5-(4-bromobenzyloxy)pentyltrifluoride

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Chemical Property of potassium 5-(4-bromobenzyloxy)pentyltrifluoride

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Technology Process of potassium 5-(4-bromobenzyloxy)pentyltrifluoride

There total 1 articles about potassium 5-(4-bromobenzyloxy)pentyltrifluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1084847-76-6
1-bromo-4-((-pent-4-enyloxy)methyl)benzene

: 1086975-29-2
potassium 5-(4-bromobenzyloxy)pentyltrifluoride

Guidance literature:: 1-bromo-4-((-pent-4-enyloxy)methyl)benzene; With bis(1,5-cyclooctadiene)diiridium(I) dichloride; 1,2-bis-(diphenylphosphino)ethane; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere;

With potassium hydrogen difluoride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja807076d

Reference yield: 71.0%

: 300-57-2,57807-91-7
allylbenzene

: 1086975-29-2
potassium 5-(4-bromobenzyloxy)pentyltrifluoride

: potassium 5-(4-(3-phenylpropyl)benzyloxy)pentyltrifluoroborate

Guidance literature:: allylbenzene; With 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;

potassium 5-(4-bromobenzyloxy)pentyltrifluoride; With potassium fluoride; palladium diacetate; DavePhos; In tetrahydrofuran; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ja807076d

Reference yield: 71.0%

: 300-57-2,57807-91-7
allylbenzene

: 1086975-29-2
potassium 5-(4-bromobenzyloxy)pentyltrifluoride

: 1086975-36-1
C₆H₅(CH₂)3C₆H₄CH₂O(CH₂)5BF₃^(1-)*K⁽¹⁺⁾=C₆H₅(CH₂)3C₆H₄CH₂O(CH₂)5BF₃K

Guidance literature:: With palladium diacetate; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; treatment of 1.1 equiv. of allylbenzene with 1.1 equiv. of borane deriv.in THF, then treatment with 3 equiv. of KF and 1 equiv. of trifluorobor ate deriv. in presence of palladium compd. and phosphine deriv. at room temp. for 4 h;
DOI:10.1021/ja807076d