C₂₅H₂₇FN₂O₅S

Base Information

Chemical Name:C₂₅H₂₇FN₂O₅S
CAS No.:1374234-03-3
Molecular Formula:C₂₅H₂₇FN₂O₅S
Molecular Weight:486.564
Hs Code.:

C<sub>25</sub>H<sub>27</sub>FN<sub>2</sub>O<sub>5</sub>S

Synonyms:C₂₅H₂₇FN₂O₅S

Suppliers and Price of C₂₅H₂₇FN₂O₅S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₅H₂₇FN₂O₅S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₅H₂₇FN₂O₅S

There total 8 articles about C₂₅H₂₇FN₂O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1374234-02-2
C₂₃H₂₅FN₂O₅S

: 247129-85-7
(2-bromoethyl)(diphenyl)sulfonium trifluoromethanesulfonate

: 1374234-03-3
C₂₅H₂₇FN₂O₅S

Guidance literature:: C₂₃H₂₅FN₂O₅S; With sodium hydride; In dichloromethane; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;

(2-bromoethyl)(diphenyl)sulfonium trifluoromethanesulfonate; In dichloromethane; mineral oil; at 0 - 20 ℃;

Reference yield:

: 691857-46-2
ethyl 2-(4-fluorophenyl)-5-hydroxy-6-nitrobenzofuran-3-carboxylate

: 1374234-03-3
C₂₅H₂₇FN₂O₅S

Guidance literature:: Multi-step reaction with 7 steps

1.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 2 h / 0 °C

2.1: triethylamine / (diphenylphosphin)ferrocene; palladium diacetate / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

3.1: hydrogenchloride; water / tetrahydrofuran / 0.25 h / 20 °C

4.1: tin(II) chloride dihdyrate / ethyl acetate / 1 h / 80 °C

4.2: 0.5 h / 20 °C

5.1: pyridine / 1 h / 0 - 20 °C

6.1: titanium(IV) isopropylate / tetrahydrofuran / 4 h / 20 °C

6.2: 20 °C

7.1: sodium hydride / dichloromethane; mineral oil / 0.5 h / 0 °C / Inert atmosphere

7.2: 0 - 20 °C

With pyridine; titanium(IV) isopropylate; hydrogenchloride; tin(II) chloride dihdyrate; water; sodium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; dmap; (diphenylphosphin)ferrocene; palladium diacetate; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; mineral oil;

Reference yield:

: 691857-07-5
ethyl 2-(4-fluorophenyl)-5-isopropoxy-6-nitrobenzofuran-3-carboxylate

: 1374234-03-3
C₂₅H₂₇FN₂O₅S

Guidance literature:: Multi-step reaction with 8 steps

1.1: boron trichloride / dichloromethane / 1 h / 0 - 20 °C

1.2: Cooling with ice

2.1: N-ethyl-N,N-diisopropylamine / dmap / dichloromethane / 2 h / 0 °C

3.1: triethylamine / (diphenylphosphin)ferrocene; palladium diacetate / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

4.1: hydrogenchloride; water / tetrahydrofuran / 0.25 h / 20 °C

5.1: tin(II) chloride dihdyrate / ethyl acetate / 1 h / 80 °C

5.2: 0.5 h / 20 °C

6.1: pyridine / 1 h / 0 - 20 °C

7.1: titanium(IV) isopropylate / tetrahydrofuran / 4 h / 20 °C

7.2: 20 °C

8.1: sodium hydride / dichloromethane; mineral oil / 0.5 h / 0 °C / Inert atmosphere

8.2: 0 - 20 °C

With pyridine; titanium(IV) isopropylate; hydrogenchloride; tin(II) chloride dihdyrate; water; boron trichloride; sodium hydride; triethylamine; N-ethyl-N,N-diisopropylamine; dmap; (diphenylphosphin)ferrocene; palladium diacetate; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; mineral oil;