2-t-butyl-8-methyl-10-phenyl-5,10-dihydrophenophosphazine 10-oxide

Base Information

• Chemical Name: 2-t-butyl-8-methyl-10-phenyl-5,10-dihydrophenophosphazine 10-oxide
• CAS No.: 123324-93-6
• Molecular Formula: C₂₃H₂₄NOP
• Molecular Weight: 361.423
• Mol file: 123324-93-6.mol

Synonyms:2-t-butyl-8-methyl-10-phenyl-5,10-dihydrophenophosphazine 10-oxide

Chemical Property of 2-t-butyl-8-methyl-10-phenyl-5,10-dihydrophenophosphazine 10-oxide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-t-butyl-8-methyl-10-phenyl-5,10-dihydrophenophosphazine 10-oxide

There total 5 articles about 2-t-butyl-8-methyl-10-phenyl-5,10-dihydrophenophosphazine 10-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

Dichlorophenylphosphine (644-97-3) + 4-tert-butyl-N-(4-methylphenyl)aniline (123324-87-8) → 2-t-butyl-8-methyl-5,10-dihydrophenophosphazine 10-oxide (123324-96-9) + 2-t-butyl-8-methyl-10-phenyl-5,10-dihydrophenophosphazine + 2-t-butyl-8-methyl-10-phenyl-5,10-dihydrophenophosphazine 10-oxide (123324-93-6) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1)

Guidance literature:

at 200 ℃; for 1h; Product distribution; Mechanism; other diarylamines and arylphosphonous dichloride; other products; other temperatures; other times;

Reference yield: 27.0%

Dichlorophenylphosphine (644-97-3) + 4-tert-butyl-N-(4-methylphenyl)aniline (123324-87-8) → 2-t-butyl-8-methyl-5,10-dihydrophenophosphazine 10-oxide (123324-96-9) + 2-t-butyl-8-methyl-10-phenyl-5,10-dihydrophenophosphazine + 2-t-butyl-8-methyl-10-phenyl-5,10-dihydrophenophosphazine 10-oxide (123324-93-6)

Guidance literature:

at 200 ℃; for 1h;

Reference yield:

1-bromo-4-tert-butylbenzene (3972-65-4) → 2-t-butyl-8-methyl-10-phenyl-5,10-dihydrophenophosphazine 10-oxide (123324-93-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) Na₂CO₃, copper carbonate, 2.) NaOH / 1.) 210-230 deg C, 7 h, 2.) water, reflux, 30 min

2: 1.) C₆H₅PCl₂, 2.) NaOH / 1.) 200 deg C, 60 min, 2.) H₂O, reflux

With sodium hydroxide; basic copper carbonate powder; sodium carbonate; Dichlorophenylphosphine;

upstream raw materials:

Dichlorophenylphosphine

4-tert-butyl-N-(4-methylphenyl)aniline

1-bromo-4-tert-butylbenzene

N-(4-methylphenyl)formamide