2-hydroxy-α-(4-methoxyphenoxy)-4-(tetra-O-acetyl-β-D-glucopyranosyloxy)acetophenone

Base Information

Chemical Name:2-hydroxy-α-(4-methoxyphenoxy)-4-(tetra-O-acetyl-β-D-glucopyranosyloxy)acetophenone
CAS No.:121361-57-7
Molecular Formula:C₂₉H₃₂O₁₄
Molecular Weight:604.565
Hs Code.:

Synonyms:2-hydroxy-α-(4-methoxyphenoxy)-4-(tetra-O-acetyl-β-D-glucopyranosyloxy)acetophenone

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Chemical Property of 2-hydroxy-α-(4-methoxyphenoxy)-4-(tetra-O-acetyl-β-D-glucopyranosyloxy)acetophenone

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Technology Process of 2-hydroxy-α-(4-methoxyphenoxy)-4-(tetra-O-acetyl-β-D-glucopyranosyloxy)acetophenone

There total 3 articles about 2-hydroxy-α-(4-methoxyphenoxy)-4-(tetra-O-acetyl-β-D-glucopyranosyloxy)acetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 121361-55-5
2,4-dihydroxy-α-(4-methoxyphenoxy)acetophenone

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 121361-57-7
2-hydroxy-α-(4-methoxyphenoxy)-4-(tetra-O-acetyl-β-D-glucopyranosyloxy)acetophenone

Guidance literature:: With potassium hydroxide; In N,N-dimethyl-formamide; acetone; for 24h; Ambient temperature;
DOI:10.1007/BF00598527

Reference yield:

: 22446-12-4
2-(4-methoxyphenoxy)acetonitrile

: 121361-57-7
2-hydroxy-α-(4-methoxyphenoxy)-4-(tetra-O-acetyl-β-D-glucopyranosyloxy)acetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 1) dry HCl, anhydrous zinc chloride, 2) water / 1) benzene, ether, 1 d, 2) 3 h, reflux

2: 45 percent / 50percent aq. potassium hydroxide / dimethylformamide; acetone / 24 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; water; zinc(II) chloride; In N,N-dimethyl-formamide; acetone;
DOI:10.1007/BF00598527

Reference yield:

: 108-46-3
recorcinol

: 121361-57-7
2-hydroxy-α-(4-methoxyphenoxy)-4-(tetra-O-acetyl-β-D-glucopyranosyloxy)acetophenone

Guidance literature:: Multi-step reaction with 2 steps

1: 1) dry HCl, anhydrous zinc chloride, 2) water / 1) benzene, ether, 1 d, 2) 3 h, reflux

2: 45 percent / 50percent aq. potassium hydroxide / dimethylformamide; acetone / 24 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; water; zinc(II) chloride; In N,N-dimethyl-formamide; acetone;
DOI:10.1007/BF00598527