Decylammonium chloride

Base Information

• Chemical Name: Decylammonium chloride
• CAS No.: 143-09-9
• Molecular Formula: C10H23 N . Cl H
• Molecular Weight: 193.76
• Mol file: 143-09-9.mol

Synonyms:decylamine;decylammonium chloride

Chemical Property of Decylammonium chloride

Chemical Property:

• Vapor Pressure: 0.107mmHg at 25°C
• Boiling Point: 221.4°Cat760mmHg
• Flash Point: 85.6°C
• Density: g/cm³
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 8
• Exact Mass: 193.1597275
• Heavy Atom Count: 12
• Complexity: 61.9

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCC[NH3+].[Cl-]

Technology Process of Decylammonium chloride

There total 5 articles about Decylammonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

n-decanenitrile (1975-78-6) → decylamine hydrochloride (143-09-9)

Guidance literature:

n-decanenitrile; With MnBr(CO)2[NH(CH₂CH₂P(iPr)2)2]; hydrogen; sodium t-butanolate; In toluene; at 120 ℃; for 36h; under 37503.8 Torr; Autoclave;

With hydrogenchloride; In diethyl ether;

DOI:10.1021/jacs.6b03709

Reference yield: 90.0%

1-azidodecane (62103-13-3) → decylamine hydrochloride (143-09-9)

Guidance literature:

1-azidodecane; With triphenylphosphine; In methanol; at 80 ℃; for 24h;

With hydrogenchloride;

DOI:10.1002/cmdc.201600400

Reference yield:

n-decanenitrile (1975-78-6) → 1-Decanol (112-30-1) + decylamine hydrochloride (143-09-9)

Guidance literature:

With hydrogenchloride; water; hydrogen; In propan-1-ol; at 80 ℃; for 3h; under 1125.11 Torr; Flow reactor;

DOI:10.1002/open.201600166

upstream raw materials:

1-aminodecane

n-decanenitrile

1-bromo dodecane

1-azidodecane

Downstream raw materials:

C₂₀H₃₃NO₄S

N₅-decyl-N₁-methyl-N₁-benzyl-biguanide

Refernces

• 1、 Schenk, K. J.,Ogle, C. A.,Chapuis, G.,Cavagnat, R.,Jokic, A.,Rey-Lafon, M.. "A Vibrational and Structural Study of the Solid-Solid Phase Transitions in C10H21NH3Cl". . p. 5040 - 5049. Retrieved 1989.
• 2、 Saito, Yuki,Ishitani, Haruro,Ueno, Masaharu,Kobayashi, Shū. "Selective Hydrogenation of Nitriles to Primary Amines Catalyzed by a Polysilane/SiO2-Supported Palladium Catalyst under Continuous-Flow Conditions". . p. 211 - 215. Retrieved 2017/04/21.