2-<5-(3-cyano-2-methyl-1-isothioureido)pentyl>-6-phenyl-3(2H)-pyridazinone

Base Information

Chemical Name:2-<5-(3-cyano-2-methyl-1-isothioureido)pentyl>-6-phenyl-3(2H)-pyridazinone
CAS No.:79460-72-3
Molecular Formula:C₁₈H₂₁N₅OS
Molecular Weight:355.464
Hs Code.:

Synonyms:2-<5-(3-cyano-2-methyl-1-isothioureido)pentyl>-6-phenyl-3(2H)-pyridazinone

Suppliers and Price of 2-<5-(3-cyano-2-methyl-1-isothioureido)pentyl>-6-phenyl-3(2H)-pyridazinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-<5-(3-cyano-2-methyl-1-isothioureido)pentyl>-6-phenyl-3(2H)-pyridazinone

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Technology Process of 2-<5-(3-cyano-2-methyl-1-isothioureido)pentyl>-6-phenyl-3(2H)-pyridazinone

There total 6 articles about 2-<5-(3-cyano-2-methyl-1-isothioureido)pentyl>-6-phenyl-3(2H)-pyridazinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 82362-85-4
2-(2-aminopentyl)-6-phenyl-3(2H)-pyridazinone

: 10191-60-3
dimethyl N-cyanodithioiminocarbonate

: 79460-72-3
2-<5-(3-cyano-2-methyl-1-isothioureido)pentyl>-6-phenyl-3(2H)-pyridazinone

Guidance literature:: In ethanol; at 0 - 5 ℃; for 2h;
DOI:10.1021/jm00357a012

Reference yield:

: 2166-31-6
6-phenylpyridazin-3(2H)-one

: 79460-72-3
2-<5-(3-cyano-2-methyl-1-isothioureido)pentyl>-6-phenyl-3(2H)-pyridazinone

Guidance literature:: Multi-step reaction with 3 steps

1: KOH, tetra-n-butylammonium bromide (TBAB) / benzene / 6 h / Ambient temperature

2: 66 percent / 28 percent amonium hydroxide / ethanol / 24 h / 40 °C

3: 76 percent / ethanol / 2 h / 0 - 5 °C

With potassium hydroxide; ammonium hydroxide; tetrabutylammomium bromide; In ethanol; benzene;
DOI:10.1021/jm00357a012

Reference yield:

: 111-24-0
1,5-dibromo-pentane

: 79460-72-3
2-<5-(3-cyano-2-methyl-1-isothioureido)pentyl>-6-phenyl-3(2H)-pyridazinone

Guidance literature:: Multi-step reaction with 3 steps

1: KOH, tetra-n-butylammonium bromide (TBAB) / benzene / 6 h / Ambient temperature

2: 66 percent / 28 percent amonium hydroxide / ethanol / 24 h / 40 °C

3: 76 percent / ethanol / 2 h / 0 - 5 °C

With potassium hydroxide; ammonium hydroxide; tetrabutylammomium bromide; In ethanol; benzene;
DOI:10.1021/jm00357a012