(1R,2R)-1-((3aS,6S,7S,7aR)-1-Benzyl-7-hydroxy-6-methyl-hexahydro-pyrano[4,3-c]isoxazol-6-yl)-propane-1,2,3-triol

Base Information

• Chemical Name: (1R,2R)-1-((3aS,6S,7S,7aR)-1-Benzyl-7-hydroxy-6-methyl-hexahydro-pyrano[4,3-c]isoxazol-6-yl)-propane-1,2,3-triol
• CAS No.: 595566-23-7
• Molecular Formula: C₁₇H₂₅NO₆
• Molecular Weight: 339.389

Synonyms:(1R,2R)-1-((3aS,6S,7S,7aR)-1-Benzyl-7-hydroxy-6-methyl-hexahydro-pyrano[4,3-c]isoxazol-6-yl)-propane-1,2,3-triol

Chemical Property of (1R,2R)-1-((3aS,6S,7S,7aR)-1-Benzyl-7-hydroxy-6-methyl-hexahydro-pyrano[4,3-c]isoxazol-6-yl)-propane-1,2,3-triol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

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Useful:

Technology Process of (1R,2R)-1-((3aS,6S,7S,7aR)-1-Benzyl-7-hydroxy-6-methyl-hexahydro-pyrano[4,3-c]isoxazol-6-yl)-propane-1,2,3-triol

There total 1 articles about (1R,2R)-1-((3aS,6S,7S,7aR)-1-Benzyl-7-hydroxy-6-methyl-hexahydro-pyrano[4,3-c]isoxazol-6-yl)-propane-1,2,3-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(3aS,6S,7S,7aR)-7-acetoxy-1-benzyl-6-methyl-6-[((1R,2R)-1,2,3-triacetoxy)prop-1-yl]-1,3,3a,6,7,7a-hexahydro-4H-pyrano[4,5-c]isoxazole (170898-58-5) → (1R,2R)-1-((3aS,6S,7S,7aR)-1-Benzyl-7-hydroxy-6-methyl-hexahydro-pyrano[4,3-c]isoxazol-6-yl)-propane-1,2,3-triol (595566-23-7)

Guidance literature:

With sodium; In methanol; at 25 ℃; for 4h;

DOI:10.1016/S0040-4020(03)00634-3

Reference yield: 65.0%

(1R,2R)-1-((3aS,6S,7S,7aR)-1-Benzyl-7-hydroxy-6-methyl-hexahydro-pyrano[4,3-c]isoxazol-6-yl)-propane-1,2,3-triol (595566-23-7) → (3aS,6S,7S,7aR)-1-Benzyl-7-hydroxy-6-methyl-hexahydro-pyrano[4,3-c]isoxazole-6-carbaldehyde (595566-35-1)

Guidance literature:

With sodium periodate; In methanol; at 25 ℃; for 2h;

DOI:10.1016/S0040-4020(03)00634-3

Reference yield: 60.0%

acetic anhydride (108-24-7) + (1R,2R)-1-((3aS,6S,7S,7aR)-1-Benzyl-7-hydroxy-6-methyl-hexahydro-pyrano[4,3-c]isoxazol-6-yl)-propane-1,2,3-triol (595566-23-7) → (3aS,6S,7S,7aR)-7-acetoxy-1-benzyl-6-methyl-6-[((1R,2R)-1,2,3-triacetoxy)prop-1-yl]-1,3,3a,6,7,7a-hexahydro-4H-pyrano[4,5-c]isoxazole (170898-58-5)

Guidance literature:

With pyridine; at 25 ℃; for 14h;

DOI:10.1016/S0040-4020(03)00634-3

upstream raw materials:

(3aS,6S,7S,7aR)-7-acetoxy-1-benzyl-6-methyl-6-[((1R,2R)-1,2,3-triacetoxy)prop-1-yl]-1,3,3a,6,7,7a-hexahydro-4H-pyrano[4,5-c]isoxazole

Downstream raw materials:

(3aS,6S,7S,7aR)-7-acetoxy-1-benzyl-6-methyl-6-[((1R,2R)-1,2,3-triacetoxy)prop-1-yl]-1,3,3a,6,7,7a-hexahydro-4H-pyrano[4,5-c]isoxazole

(3aS,6S,7S,7aR)-1-Benzyl-7-hydroxy-6-methyl-hexahydro-pyrano[4,3-c]isoxazole-6-carbaldehyde

(3aS,6R,7S,7aR)-1-Benzyl-6-hydroxymethyl-6-methyl-hexahydro-pyrano[4,3-c]isoxazol-7-ol

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