(3-benzyloxy-4-methoxyphenyl)(2-β-<(N,N-dimethyl)aminoethyl>-4,5-methylenedioxyphenyl)-ethanedione

Base Information

Chemical Name:(3-benzyloxy-4-methoxyphenyl)(2-β-<(N,N-dimethyl)aminoethyl>-4,5-methylenedioxyphenyl)-ethanedione
CAS No.:124465-50-5
Molecular Formula:C₂₇H₂₇NO₆
Molecular Weight:461.514
Hs Code.:

Synonyms:(3-benzyloxy-4-methoxyphenyl)(2-β-<(N,N-dimethyl)aminoethyl>-4,5-methylenedioxyphenyl)-ethanedione

Suppliers and Price of (3-benzyloxy-4-methoxyphenyl)(2-β-<(N,N-dimethyl)aminoethyl>-4,5-methylenedioxyphenyl)-ethanedione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (3-benzyloxy-4-methoxyphenyl)(2-β-<(N,N-dimethyl)aminoethyl>-4,5-methylenedioxyphenyl)-ethanedione

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3-benzyloxy-4-methoxyphenyl)(2-β-<(N,N-dimethyl)aminoethyl>-4,5-methylenedioxyphenyl)-ethanedione

There total 4 articles about (3-benzyloxy-4-methoxyphenyl)(2-β-<(N,N-dimethyl)aminoethyl>-4,5-methylenedioxyphenyl)-ethanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60229-32-5
[2-(6-formyl-benzo[1,3]dioxol-5-yl)-ethyl]-methyl-carbamic acid ethyl ester

: 124465-50-5
(3-benzyloxy-4-methoxyphenyl)(2-β-<(N,N-dimethyl)aminoethyl>-4,5-methylenedioxyphenyl)-ethanedione

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / 50percent sodium hydroxide, TEBA / benzene / 5 h / Ambient temperature

2: 67 percent / lithium aluminium hydride / tetrahydrofuran / 5 h / Ambient temperature

3: 1.) oxalyl chloride, DMSO, 2.) triethylamine / 1.) dichloromethane, -60 deg C, 15 min, 2.) dichloromethane, -60 deg C

With sodium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; N-benzyl-N,N,N-triethylammonium chloride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; benzene;

Reference yield:

: 124465-47-0
2-benzoyloxy-2-(3'-benzyloxy-4'-methoxy)acetonitrile

: 124465-50-5
(3-benzyloxy-4-methoxyphenyl)(2-β-<(N,N-dimethyl)aminoethyl>-4,5-methylenedioxyphenyl)-ethanedione

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / 50percent sodium hydroxide, TEBA / benzene / 5 h / Ambient temperature

2: 67 percent / lithium aluminium hydride / tetrahydrofuran / 5 h / Ambient temperature

3: 1.) oxalyl chloride, DMSO, 2.) triethylamine / 1.) dichloromethane, -60 deg C, 15 min, 2.) dichloromethane, -60 deg C

With sodium hydroxide; lithium aluminium tetrahydride; oxalyl dichloride; N-benzyl-N,N,N-triethylammonium chloride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; benzene;

Reference yield:

: 124465-48-1
2-benzoyloxy-1-(3-benzyloxy-4-methoxyphenyl)-2-<2-β-(N-ethoxycarbonyl-N-methyl)aminoethyl>-4,5-methylenedioxy-phenylethanone

: 124465-50-5
(3-benzyloxy-4-methoxyphenyl)(2-β-<(N,N-dimethyl)aminoethyl>-4,5-methylenedioxyphenyl)-ethanedione

Guidance literature:: Multi-step reaction with 2 steps

1: 67 percent / lithium aluminium hydride / tetrahydrofuran / 5 h / Ambient temperature

2: 1.) oxalyl chloride, DMSO, 2.) triethylamine / 1.) dichloromethane, -60 deg C, 15 min, 2.) dichloromethane, -60 deg C

With lithium aluminium tetrahydride; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran;