N,N'-bis-(3-amino-5-dioctylcarbamoyl-2-fluoro-phenyl)-2-fluoro-isophthalamide

Base Information

Chemical Name:N,N'-bis-(3-amino-5-dioctylcarbamoyl-2-fluoro-phenyl)-2-fluoro-isophthalamide
CAS No.:869203-28-1
Molecular Formula:C₅₄H₈₁F₃N₆O₄
Molecular Weight:935.27
Hs Code.:

<i>N</i>,<i>N</i>'-bis-(3-amino-5-dioctylcarbamoyl-2-fluoro-phenyl)-2-fluoro-isophthalamide

Synonyms:N,N'-bis-(3-amino-5-dioctylcarbamoyl-2-fluoro-phenyl)-2-fluoro-isophthalamide

Suppliers and Price of N,N'-bis-(3-amino-5-dioctylcarbamoyl-2-fluoro-phenyl)-2-fluoro-isophthalamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N,N'-bis-(3-amino-5-dioctylcarbamoyl-2-fluoro-phenyl)-2-fluoro-isophthalamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N,N'-bis-(3-amino-5-dioctylcarbamoyl-2-fluoro-phenyl)-2-fluoro-isophthalamide

There total 5 articles about N,N'-bis-(3-amino-5-dioctylcarbamoyl-2-fluoro-phenyl)-2-fluoro-isophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 869203-26-9
4-fluoro-3,5-dinitro-N,N-dioctyl-benzamide

: 869203-28-1
N,N'-bis-(3-amino-5-dioctylcarbamoyl-2-fluoro-phenyl)-2-fluoro-isophthalamide

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / H₂ / Pd/C / methanol; tetrahydrofuran / 48 h / 20 °C / 760 Torr

2: 0.40 g / Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/anie.200500982

Reference yield:

: 2365-73-3
4-fluoro-3,5-dinitro-benzoyl chloride

: 869203-28-1
N,N'-bis-(3-amino-5-dioctylcarbamoyl-2-fluoro-phenyl)-2-fluoro-isophthalamide

Guidance literature:: Multi-step reaction with 3 steps

1: 3.21 g / Et₃N / tetrahydrofuran / 1 h / -10 °C

2: 92 percent / H₂ / Pd/C / methanol; tetrahydrofuran / 48 h / 20 °C / 760 Torr

3: 0.40 g / Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/anie.200500982

Reference yield:

: 2365-71-1
3,5-dinitro-4-fluorobenzoic acid

: 869203-28-1
N,N'-bis-(3-amino-5-dioctylcarbamoyl-2-fluoro-phenyl)-2-fluoro-isophthalamide

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl chloride; DMF / tetrahydrofuran / 0.5 h / 20 °C

2: 3.21 g / Et₃N / tetrahydrofuran / 1 h / -10 °C

3: 92 percent / H₂ / Pd/C / methanol; tetrahydrofuran / 48 h / 20 °C / 760 Torr

4: 0.40 g / Et₃N / CH₂Cl₂ / 0.5 h / 20 °C

With oxalyl dichloride; hydrogen; triethylamine; N,N-dimethyl-formamide; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1002/anie.200500982