1,1-di(p-methoxyphenyl)-3-phenylpropargyl alcohol

Base Information

Chemical Name:1,1-di(p-methoxyphenyl)-3-phenylpropargyl alcohol
CAS No.:548796-81-2
Molecular Formula:C₂₃H₂₀O₃
Molecular Weight:344.41
Hs Code.:

Synonyms:1,1-di(p-methoxyphenyl)-3-phenylpropargyl alcohol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-di(p-methoxyphenyl)-3-phenylpropargyl alcohol

Chemical Property:

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Technology Process of 1,1-di(p-methoxyphenyl)-3-phenylpropargyl alcohol

There total 2 articles about 1,1-di(p-methoxyphenyl)-3-phenylpropargyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 90-96-0
bis(p-methoxyphenyl)methanone

: 536-74-3
phenylacetylene

: 548796-81-2
1,1-di(p-methoxyphenyl)-3-phenylpropargyl alcohol

Guidance literature:: phenylacetylene; With n-butyllithium; In tetrahydrofuran; hexanes; at -78 ℃; Inert atmosphere;

bis(p-methoxyphenyl)methanone; In tetrahydrofuran; hexanes; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1039/c0ob00141d

Reference yield:

: 90-96-0
bis(p-methoxyphenyl)methanone

: 4440-01-1
lithium phenylacetylide

: 548796-81-2
1,1-di(p-methoxyphenyl)-3-phenylpropargyl alcohol

Guidance literature:

Reference yield: 98.0%

: 548796-81-2
1,1-di(p-methoxyphenyl)-3-phenylpropargyl alcohol

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 3,4-bis(4-methoxyphenyl)-5-phenyl-1H-pyrazole

Guidance literature:: 1,1-di(p-methoxyphenyl)-3-phenylpropargyl alcohol; toluene-4-sulfonic acid hydrazide; With iron(III) chloride; In chlorobenzene; at 60 ℃; for 1h;

With caesium carbonate; In chlorobenzene; at 100 ℃; for 3h; regioselective reaction;
DOI:10.1002/chem.201204322