N-(4-methylphenyl)-3,5-dinitrobenzamide

Base Information

• Chemical Name: N-(4-methylphenyl)-3,5-dinitrobenzamide
• CAS No.: 92164-94-8
• Molecular Formula: C₁₄H₁₁N₃O₅
• Molecular Weight: 301.258
• Mol file: 92164-94-8.mol

Synonyms:3,5-dinitro-benzoic acid p-toluidide

Chemical Property of N-(4-methylphenyl)-3,5-dinitrobenzamide

Chemical Property:

Purity/Quality:

N-(4-methylphenyl)-3,5-dinitrobenzamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-(4-methylphenyl)-3,5-dinitrobenzamide

There total 3 articles about N-(4-methylphenyl)-3,5-dinitrobenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-toluidine (106-49-0,12221-03-3) + 3,5-dinitrobenoyl chloride (99-33-2) → 3,5-dinitro-benzoic acid p-toluidide (92164-94-8)

Guidance literature:

With tetralin;

Reference yield:

3,5-dinitrobenzoic acid (99-34-3) → 3,5-dinitro-benzoic acid p-toluidide (92164-94-8)

Guidance literature:

Multi-step reaction with 2 steps

1: thionyl chloride / N,N-dimethyl-formamide / 90 °C

2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 20 °C

With thionyl chloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1002/cbdv.201900304

Reference yield:

→ 3,5-dinitro-benzoic acid p-toluidide (92164-94-8)

Guidance literature:

aus dem entspr.Amin;

DOI:10.1021/je60053a005

upstream raw materials:

p-toluidine

3,5-dinitrobenoyl chloride

3,5-dinitrobenzoic acid

Downstream raw materials:

4-methyl-2,6-dinitroaniline

3,5-dinitro-benzoic acid-(4-methyl-2,6-dinitro-anilide)

Refernces