5-((E)-2-Benzenesulfonyl-vinyloxy)-hexaneselenoic acid Se-phenyl ester

Base Information

Chemical Name:5-((E)-2-Benzenesulfonyl-vinyloxy)-hexaneselenoic acid Se-phenyl ester
CAS No.:199862-45-8
Molecular Formula:C₂₀H₂₂O₄SSe
Molecular Weight:437.418
Hs Code.:

Synonyms:5-((E)-2-Benzenesulfonyl-vinyloxy)-hexaneselenoic acid Se-phenyl ester

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Chemical Property of 5-((E)-2-Benzenesulfonyl-vinyloxy)-hexaneselenoic acid Se-phenyl ester

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Technology Process of 5-((E)-2-Benzenesulfonyl-vinyloxy)-hexaneselenoic acid Se-phenyl ester

There total 4 articles about 5-((E)-2-Benzenesulfonyl-vinyloxy)-hexaneselenoic acid Se-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34837-55-3
Phenylselenyl bromide

: 285545-68-8
5-((E)-2-Benzenesulfonyl-vinyloxy)-hexanoic acid

: 199862-45-8
5-((E)-2-Benzenesulfonyl-vinyloxy)-hexaneselenoic acid Se-phenyl ester

Guidance literature:: 5-((E)-2-Benzenesulfonyl-vinyloxy)-hexanoic acid; With triethylamine; In dichloromethane; at 20 ℃; for 0.333333h;

Phenylselenyl bromide; With triethylammonium salt; tributylphosphine; In tetrahydrofuran; at 20 ℃; for 19h; Further stages.;
DOI:10.1021/jo991970b

Reference yield:

: 963-16-6
(E)-1,2-bis(phenylsulfonyl)ethylene

: 199862-45-8
5-((E)-2-Benzenesulfonyl-vinyloxy)-hexaneselenoic acid Se-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 96 percent / lithium hexamethyldisilylazide / tetrahydrofuran / 1.5 h / 20 °C

2.1: Jones reagent / acetone; H₂O / 16 h / 20 °C

3.1: trietnylamine / CH₂Cl₂ / 0.33 h / 20 °C

3.2: tributylphosphine; triethylammonium salt / tetrahydrofuran / 19 h / 20 °C

With jones reagent; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; water; acetone; 1.1: Alkylation / 2.1: Oxidation / 3.1: Substitution / 3.2: Substitution;
DOI:10.1021/jo991970b

Reference yield:

: 138611-32-2
6-<<(1,1-dimethylethyl)dimethylsilyl>oxy>-2-hexanol

: 199862-45-8
5-((E)-2-Benzenesulfonyl-vinyloxy)-hexaneselenoic acid Se-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: 96 percent / lithium hexamethyldisilylazide / tetrahydrofuran / 1.5 h / 20 °C

2.1: Jones reagent / acetone; H₂O / 16 h / 20 °C

3.1: trietnylamine / CH₂Cl₂ / 0.33 h / 20 °C

3.2: tributylphosphine; triethylammonium salt / tetrahydrofuran / 19 h / 20 °C

With jones reagent; triethylamine; lithium hexamethyldisilazane; In tetrahydrofuran; dichloromethane; water; acetone; 1.1: Alkylation / 2.1: Oxidation / 3.1: Substitution / 3.2: Substitution;
DOI:10.1021/jo991970b