(S)-2,2'-(1-(4-methoxyphenyl)ethane-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Base Information

Chemical Name:(S)-2,2'-(1-(4-methoxyphenyl)ethane-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)
CAS No.:1198172-06-3
Molecular Formula:C₂₁H₃₄B₂O₅
Molecular Weight:388.12
Hs Code.:

Synonyms:(S)-2,2'-(1-(4-methoxyphenyl)ethane-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2,2'-(1-(4-methoxyphenyl)ethane-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

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Technology Process of (S)-2,2'-(1-(4-methoxyphenyl)ethane-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

There total 2 articles about (S)-2,2'-(1-(4-methoxyphenyl)ethane-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1198171-95-7
p-MeO-C₆H₄C(Bpin)CH(Bpin)

: 1326719-63-4
(R)-2,2'-(1-(4-methoxyphenyl)ethane-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: 1198172-06-3
(S)-2,2'-(1-(4-methoxyphenyl)ethane-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Guidance literature:: With C₃₂H₁₂BF₂₄^(1-)*C₃₅H₃₈IrN₂PS⁽¹⁺⁾; hydrogen; In dichloromethane; at 20 ℃; for 18h; under 750.075 Torr; optical yield given as %ee; enantioselective reaction;
DOI:10.1039/b912590f

Reference yield:

: 1198171-95-7
p-MeO-C₆H₄C(Bpin)CH(Bpin)

: 1198172-06-3
(S)-2,2'-(1-(4-methoxyphenyl)ethane-1,2-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

Guidance literature:: With C₄₃H₆₀IrNO₃P⁽¹⁺⁾*C₃₂H₁₂BF₂₄^(1-); hydrogen; In dichloromethane; at 20 ℃; for 2h; under 37503.8 Torr; enantioselective reaction; Inert atmosphere; Schlenk technique; Autoclave;
DOI:10.1002/adsc.201201017