C₂₈H₂₃FN₅P

Base Information

• Chemical Name: C₂₈H₂₃FN₅P
• CAS No.: 1400820-30-5
• Molecular Formula: C₂₈H₂₃FN₅P
• Molecular Weight: 479.496
• Mol file: 1400820-30-5.mol

Synonyms:C₂₈H₂₃FN₅P

Chemical Property of C₂₈H₂₃FN₅P

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₈H₂₃FN₅P

There total 2 articles about C₂₈H₂₃FN₅P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C28H21FN5O2P (1400820-23-6) → C28H23FN5P (1400820-30-5)

Guidance literature:

With 5% Pd/C; hydrogen; In methanol; ethyl acetate; at 20 ℃; for 16h; under 3040.2 Torr;

DOI:10.1016/j.tetlet.2012.07.106

Reference yield:

(chloropyrazin-2-yl)imino-triphenyl-λ5-phosphane (1400820-08-7) → C28H23FN5P (1400820-30-5)

Guidance literature:

Multi-step reaction with 2 steps

1: caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; palladium diacetate / toluene / 16 h / 100 °C / Inert atmosphere

2: 5% Pd/C; hydrogen / ethyl acetate; methanol / 16 h / 20 °C / 3040.2 Torr

With 5% Pd/C; hydrogen; palladium diacetate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; In methanol; ethyl acetate; toluene;

DOI:10.1016/j.tetlet.2012.07.106

Reference yield:

C28H23FN5P (1400820-30-5) + isopentyl nitrite (110-46-3) → C28H20FN6P (1400820-36-1)

Guidance literature:

With acetic acid; at 0 - 20 ℃;

DOI:10.1016/j.tetlet.2012.07.106

upstream raw materials:

(chloropyrazin-2-yl)imino-triphenyl-λ⁵-phosphane

C₂₈H₂₁FN₅O₂P

Downstream raw materials:

C₂₈H₂₀FN₆P

Refernces