(1α,1aβ,6α,6aβ)-1,1a,6,6a-tetrahydro-1-methyl-1a,6a-diphenyl-1,6-methanocyclopropindene

Base Information

• Chemical Name: (1α,1aβ,6α,6aβ)-1,1a,6,6a-tetrahydro-1-methyl-1a,6a-diphenyl-1,6-methanocycloprop
• Molecular Formula: C₂₄H₂₀
• Molecular Weight: 308.423

Synonyms:(1α,1aβ,6α,6aβ)-1,1a,6,6a-tetrahydro-1-methyl-1a,6a-diphenyl-1,6-methanocyclopropindene

Chemical Property of (1α,1aβ,6α,6aβ)-1,1a,6,6a-tetrahydro-1-methyl-1a,6a-diphenyl-1,6-methanocycloprop

Chemical Property:

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There total 4 articles about (1α,1aβ,6α,6aβ)-1,1a,6,6a-tetrahydro-1-methyl-1a,6a-diphenyl-1,6-methanocyclopropindene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1,3-diphenyl-2-methyl-3-(o-vinylphenyl)cyclopropene (70913-11-0) → (1α,1aβ,6α,6aβ)-1,1a,6,6a-tetrahydro-1-methyl-1a,6a-diphenyl-1,6-methanocyclopropindene (80949-68-4)

Guidance literature:

In pyridine; benzene; at 175 ℃; for 0.75h;

DOI:10.1021/ja00351a051

Reference yield: 46.0%

1,3-diphenyl-2-methyl-3-(o-vinylphenyl)cyclopropene (70913-11-0) → (1α,1aβ,6α,6aβ)-1,1a,6,6a-tetrahydro-1-methyl-1a,6a-diphenyl-1,6-methanocyclopropindene (80949-68-4) + 4b,4c,9b,9c-tetrahydro-4c-methyl-9c-phenyl-5H-benzocyclopropafluorene (80949-70-8)

Guidance literature:

With thio-xanthene-9-one; In benzene; for 2h; Irradiation;

DOI:10.1021/ja00351a051

Reference yield:

1,4-dihydro-1-methyl-2,3-diphenyl-1,4-methanonaphthalene (70913-12-1) → (1α,1aβ,6α,6aβ)-1,1a,6,6a-tetrahydro-1-methyl-1a,6a-diphenyl-1,6-methanocyclopropindene (80949-68-4)

Guidance literature:

Irradiation;

DOI:10.1021/ja00351a051

upstream raw materials:

1,3-diphenyl-2-methyl-3-(o-vinylphenyl)cyclopropene

1,4-dihydro-1-methyl-2,3-diphenyl-1,4-methanonaphthalene

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